Crystallography Open Database

Information card for entry 4310468

Preview

Coordinates	4310468.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H58 Li N2 P
Calculated formula	C48 H58 Li N2 P
Title of publication	Synthesis and Structures of Complexes Demonstrating the Coordinative Versatility of the 2,4-Diimino-3-phosphinopentene Anion (γ-Phosphino-β-diketiminate)
Authors of publication	Neil Burford; Mark D'eon; Paul J. Ragogna; Robert McDonald; Michael J. Ferguson
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	734 - 738
a	10.1138 ± 0.0004 Å
b	11.1175 ± 0.0005 Å
c	19.6442 ± 0.0009 Å
α	77.193 ± 0.001°
β	84.797 ± 0.001°
γ	78.208 ± 0.001°
Cell volume	2106.01 ± 0.16 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0612
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.1217
Weighted residual factors for all reflections included in the refinement	0.1312
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179143 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/04.	4310468.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310468.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310468.cif
1956	2010-11-07	../uploads/cif-deposit/cod/cif Adding structures of 4310468 via cif-deposit CGI script.	4310468.cif