Crystallography Open Database

Information card for entry 4310591

Preview

Coordinates	4310591.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H15 Cl4 F3 Fe2 N4 O0.5
Calculated formula	C18 H15 Cl4 F3 Fe2 N4 O0.5
Title of publication	Easy Preparation of the Tris(2-fluoro-6-pyridylmethyl)amine Ligand and Instantaneous Reaction of the Corresponding Dichloroferrous Complex with Molecular Dioxygen: New Access to Dinuclear Species
Authors of publication	Ahmed Machkour; Dominique Mandon; Mohamed Lachkar; Richard Welter
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	1545 - 1550
a	9.343 ± 0.005 Å
b	9.569 ± 0.005 Å
c	13.696 ± 0.005 Å
α	102.621 ± 0.005°
β	93.289 ± 0.005°
γ	105.61 ± 0.005°
Cell volume	1142 ± 1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1516
Residual factor for significantly intense reflections	0.0829
Weighted residual factors for significantly intense reflections	0.129
Weighted residual factors for all reflections included in the refinement	0.1481
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4310591.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310591.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310591.cif
2079	2010-11-08	../uploads/cif-deposit/cod/cif Adding structures of 4310591 via cif-deposit CGI script.	4310591.cif