Crystallography Open Database

Information card for entry 4310601

Preview

Coordinates	4310601.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H73.93 B Cl0.08 N2 O9 P3 Ru
Calculated formula	C52 H73.938 B Cl0.062 N2 O9 P3 Ru
Title of publication	Preparation and Reactivity of Mixed-Ligand Ruthenium(II) Hydride Complexes with Phosphites and Polypyridyls
Authors of publication	Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Claudia D'Este; Giancarlo Pelizzi
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	1336 - 1349
a	11.415 ± 0.001 Å
b	13.98 ± 0.001 Å
c	17.751 ± 0.001 Å
α	90.832 ± 0.002°
β	91.227 ± 0.002°
γ	90.481 ± 0.002°
Cell volume	2831.7 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0729
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.1156
Weighted residual factors for all reflections included in the refinement	0.1318
Goodness-of-fit parameter for all reflections included in the refinement	1.129
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179145 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/06.	4310601.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310601.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310601.cif
2089	2010-11-08	../uploads/cif-deposit/cod/cif Adding structures of 4310601 via cif-deposit CGI script.	4310601.cif