Crystallography Open Database

Information card for entry 4310603

Preview

Coordinates	4310603.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C123 H126 Au2 Cl6 F16 N2 O9 P2 Rh4 S4
Calculated formula	C99 H60 Au2 Cl6 F16 N2 O9 P2 Rh4 S4
Title of publication	Tetranuclear [Rh4(μ-PyS2)2(diolefin)4] Complexes as Building Blocks for New Inorganic Architectures: Synthesis of Coordination Polymers and Heteropolynuclear Complexes with Electrophilic d8 and d10 Metal Fragments
Authors of publication	Miguel A. Casado; Jesús J. Pérez-Torrente; Miguel A. Ciriano; Fernando J. Lahoz; Luis A. Oro
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	1558 - 1567
a	22.7939 ± 0.0012 Å
b	21.9335 ± 0.0011 Å
c	24.5094 ± 0.0012 Å
α	90°
β	115.269 ± 0.001°
γ	90°
Cell volume	11081 ± 1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	10
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1018
Residual factor for significantly intense reflections	0.0548
Weighted residual factors for significantly intense reflections	0.1037
Weighted residual factors for all reflections included in the refinement	0.1111
Goodness-of-fit parameter for all reflections included in the refinement	0.83
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179145 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/06.	4310603.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310603.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310603.cif
2091	2010-11-08	../uploads/cif-deposit/cod/cif Adding structures of 4310603 via cif-deposit CGI script.	4310603.cif