#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:32:23 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179145 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/06/4310637.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4310637
loop_
_publ_author_name
'J. R. Salvador'
'J. R. Gour'
'D. Bilc'
'S. D. Mahanti'
'M. G. Kanatzidis'
_publ_section_title
;
 Stabilization of New Forms of the Intermetallic Phases β-RENiGe2 (RE =
 Dy, Ho, Er, Tm, Yb, Lu) in Liquid Indium
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1403
_journal_page_last               1410
_journal_paper_doi               10.1021/ic035303j
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'Dy Ge2 Ni'
_chemical_formula_weight         366.39
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   4.1784(9)
_cell_length_b                   8.8645(19)
_cell_length_c                   15.745(3)
_cell_measurement_temperature    293(2)
_cell_volume                     583.2(2)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0517
_diffrn_reflns_av_sigmaI/netI    0.0258
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            2522
_diffrn_reflns_theta_full        27.01
_diffrn_reflns_theta_max         27.01
_diffrn_reflns_theta_min         2.59
_exptl_absorpt_coefficient_mu    51.676
_exptl_crystal_density_diffrn    8.437
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             632
_refine_diff_density_max         3.984
_refine_diff_density_min         -4.443
_refine_diff_density_rms         0.947
_refine_ls_extinction_coef       0.0019(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.266
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     30
_refine_ls_number_reflns         401
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.266
_refine_ls_R_factor_all          0.0429
_refine_ls_R_factor_gt           0.0421
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0685P)²+33.9381P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1174
_refine_ls_wR_factor_ref         0.1181
_reflns_number_gt                390
_reflns_number_total             401
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic035303jsi20031111_122754_1.cif
_cod_data_source_block           dynige2m
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4310637
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.0000 0.5000 0.20813(7) 0.0053(4) Uani 1 4 d S . .
Dy2 Dy 0.0000 0.28309(13) 0.0000 0.0069(5) Uani 1 4 d S . .
Ge1 Ge 0.0000 0.5000 0.41432(12) 0.0114(7) Uani 1 4 d S . .
Ge2 Ge 0.5000 0.5000 0.07863(16) 0.0062(6) Uani 1 4 d S . .
Ge3 Ge 0.0000 0.1591(2) 0.19068(11) 0.0073(5) Uani 1 2 d S . .
Ni1 Ni 0.0000 0.2352(3) 0.34660(14) 0.0075(6) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge2 Dy1 Ge2 91.39(8) . 1_455 ?
Ge2 Dy1 Ge3 82.63(4) . 13 ?
Ge2 Dy1 Ge3 150.99(4) 1_455 13 ?
Ge2 Dy1 Ge3 150.99(4) . 13_455 ?
Ge2 Dy1 Ge3 82.63(4) 1_455 13_455 ?
Ge3 Dy1 Ge3 88.95(5) 13 13_455 ?
Ge2 Dy1 Ge3 82.63(4) . 14 ?
Ge2 Dy1 Ge3 150.99(4) 1_455 14 ?
Ge3 Dy1 Ge3 56.46(7) 13 14 ?
Ge3 Dy1 Ge3 115.41(7) 13_455 14 ?
Ge2 Dy1 Ge3 150.99(4) . 14_455 ?
Ge2 Dy1 Ge3 82.63(4) 1_455 14_455 ?
Ge3 Dy1 Ge3 115.41(7) 13 14_455 ?
Ge3 Dy1 Ge3 56.46(7) 13_455 14_455 ?
Ge3 Dy1 Ge3 88.95(5) 14 14_455 ?
Ge2 Dy1 Ge3 86.37(3) . . ?
Ge2 Dy1 Ge3 86.38(3) 1_455 . ?
Ge3 Dy1 Ge3 64.99(4) 13 . ?
Ge3 Dy1 Ge3 64.99(4) 13_455 . ?
Ge3 Dy1 Ge3 121.30(4) 14 . ?
Ge3 Dy1 Ge3 121.30(4) 14_455 . ?
Ge2 Dy1 Ge3 86.37(3) . 2_565 ?
Ge2 Dy1 Ge3 86.37(3) 1_455 2_565 ?
Ge3 Dy1 Ge3 121.30(4) 13 2_565 ?
Ge3 Dy1 Ge3 121.30(4) 13_455 2_565 ?
Ge3 Dy1 Ge3 64.99(4) 14 2_565 ?
Ge3 Dy1 Ge3 64.99(4) 14_455 2_565 ?
Ge3 Dy1 Ge3 169.61(8) . 2_565 ?
Ge2 Dy1 Ni1 106.89(5) . 13_455 ?
Ge2 Dy1 Ni1 47.00(4) 1_455 13_455 ?
Ge3 Dy1 Ni1 107.76(5) 13 13_455 ?
Ge3 Dy1 Ni1 49.68(5) 13_455 13_455 ?
Ge3 Dy1 Ni1 161.18(6) 14 13_455 ?
Ge3 Dy1 Ni1 89.68(4) 14_455 13_455 ?
Ge3 Dy1 Ni1 45.52(3) . 13_455 ?
Ge3 Dy1 Ni1 130.53(4) 2_565 13_455 ?
Ge2 Dy1 Ni1 47.00(4) . 13 ?
Ge2 Dy1 Ni1 106.89(5) 1_455 13 ?
Ge3 Dy1 Ni1 49.68(5) 13 13 ?
Ge3 Dy1 Ni1 107.76(5) 13_455 13 ?
Ge3 Dy1 Ni1 89.68(4) 14 13 ?
Ge3 Dy1 Ni1 161.18(6) 14_455 13 ?
Ge3 Dy1 Ni1 45.52(3) . 13 ?
Ge3 Dy1 Ni1 130.53(4) 2_565 13 ?
Ni1 Dy1 Ni1 85.61(6) 13_455 13 ?
Ge2 Dy1 Ni1 47.00(4) . 14 ?
Ge2 Dy1 Ni1 106.89(5) 1_455 14 ?
Ge3 Dy1 Ni1 89.68(4) 13 14 ?
Ge3 Dy1 Ni1 161.17(6) 13_455 14 ?
Ge3 Dy1 Ni1 49.68(5) 14 14 ?
Ge3 Dy1 Ni1 107.76(5) 14_455 14 ?
Ge3 Dy1 Ni1 130.53(4) . 14 ?
Ge3 Dy1 Ni1 45.52(3) 2_565 14 ?
Ni1 Dy1 Ni1 147.45(9) 13_455 14 ?
Ni1 Dy1 Ni1 85.38(7) 13 14 ?
Ge2 Dy1 Ni1 106.89(5) . 14_455 ?
Ge2 Dy1 Ni1 47.00(4) 1_455 14_455 ?
Ge3 Dy1 Ni1 161.17(6) 13 14_455 ?
Ge3 Dy1 Ni1 89.68(4) 13_455 14_455 ?
Ge3 Dy1 Ni1 107.76(5) 14 14_455 ?
Ge3 Dy1 Ni1 49.68(5) 14_455 14_455 ?
Ge3 Dy1 Ni1 130.53(4) . 14_455 ?
Ge3 Dy1 Ni1 45.52(3) 2_565 14_455 ?
Ni1 Dy1 Ni1 85.38(7) 13_455 14_455 ?
Ni1 Dy1 Ni1 147.45(9) 13 14_455 ?
Ni1 Dy1 Ni1 85.61(6) 14 14_455 ?
Ge2 Dy2 Ge2 47.12(9) . 9_665 ?
Ge2 Dy2 Ge2 103.26(5) . 9_565 ?
Ge2 Dy2 Ge2 84.83(4) 9_665 9_565 ?
Ge2 Dy2 Ge2 84.83(4) . 1_455 ?
Ge2 Dy2 Ge2 103.26(5) 9_665 1_455 ?
Ge2 Dy2 Ge2 47.12(9) 9_565 1_455 ?
Ge2 Dy2 Ge3 126.06(5) . 10 ?
Ge2 Dy2 Ge3 80.68(5) 9_665 10 ?
Ge2 Dy2 Ge3 80.68(5) 9_565 10 ?
Ge2 Dy2 Ge3 126.06(5) 1_455 10 ?
Ge2 Dy2 Ge3 80.68(5) . . ?
Ge2 Dy2 Ge3 126.06(5) 9_665 . ?
Ge2 Dy2 Ge3 126.06(5) 9_565 . ?
Ge2 Dy2 Ge3 80.68(5) 1_455 . ?
Ge3 Dy2 Ge3 139.80(8) 10 . ?
Ge2 Dy2 Ni1 140.72(6) . 6_454 ?
Ge2 Dy2 Ni1 99.80(5) 9_665 6_454 ?
Ge2 Dy2 Ni1 44.67(5) 9_565 6_454 ?
Ge2 Dy2 Ni1 83.84(6) 1_455 6_454 ?
Ge3 Dy2 Ni1 43.39(3) 10 6_454 ?
Ge3 Dy2 Ni1 133.78(4) . 6_454 ?
Ge2 Dy2 Ni1 44.67(5) . 13 ?
Ge2 Dy2 Ni1 83.84(6) 9_665 13 ?
Ge2 Dy2 Ni1 140.72(6) 9_565 13 ?
Ge2 Dy2 Ni1 99.80(5) 1_455 13 ?
Ge3 Dy2 Ni1 133.78(4) 10 13 ?
Ge3 Dy2 Ni1 43.39(3) . 13 ?
Ni1 Dy2 Ni1 174.19(9) 6_454 13 ?
Ge2 Dy2 Ni1 83.84(6) . 6_554 ?
Ge2 Dy2 Ni1 44.67(5) 9_665 6_554 ?
Ge2 Dy2 Ni1 99.80(5) 9_565 6_554 ?
Ge2 Dy2 Ni1 140.72(6) 1_455 6_554 ?
Ge3 Dy2 Ni1 43.39(3) 10 6_554 ?
Ge3 Dy2 Ni1 133.78(4) . 6_554 ?
Ni1 Dy2 Ni1 81.59(6) 6_454 6_554 ?
Ni1 Dy2 Ni1 98.11(6) 13 6_554 ?
Ge2 Dy2 Ni1 99.80(5) . 13_455 ?
Ge2 Dy2 Ni1 140.72(6) 9_665 13_455 ?
Ge2 Dy2 Ni1 83.84(6) 9_565 13_455 ?
Ge2 Dy2 Ni1 44.67(5) 1_455 13_455 ?
Ge3 Dy2 Ni1 133.78(4) 10 13_455 ?
Ge3 Dy2 Ni1 43.39(3) . 13_455 ?
Ni1 Dy2 Ni1 98.11(6) 6_454 13_455 ?
Ni1 Dy2 Ni1 81.59(6) 13 13_455 ?
Ni1 Dy2 Ni1 174.19(9) 6_554 13_455 ?
Ge2 Dy2 Dy1 48.79(4) . . ?
Ge2 Dy2 Dy1 91.75(5) 9_665 . ?
Ge2 Dy2 Dy1 91.75(5) 9_565 . ?
Ge2 Dy2 Dy1 48.79(4) 1_455 . ?
Ge3 Dy2 Dy1 169.70(5) 10 . ?
Ge3 Dy2 Dy1 50.50(4) . . ?
Ni1 Dy2 Dy1 132.62(4) 6_454 . ?
Ni1 Dy2 Dy1 51.26(4) 13 . ?
Ni1 Dy2 Dy1 132.62(4) 6_554 . ?
Ni1 Dy2 Dy1 51.26(4) 13_455 . ?
Ge2 Dy2 Dy1 91.75(5) . 9_565 ?
Ge2 Dy2 Dy1 48.79(4) 9_665 9_565 ?
Ge2 Dy2 Dy1 48.79(4) 9_565 9_565 ?
Ge2 Dy2 Dy1 91.75(5) 1_455 9_565 ?
Ge3 Dy2 Dy1 50.50(4) 10 9_565 ?
Ge3 Dy2 Dy1 169.70(5) . 9_565 ?
Ni1 Dy2 Dy1 51.26(4) 6_454 9_565 ?
Ni1 Dy2 Dy1 132.62(4) 13 9_565 ?
Ni1 Dy2 Dy1 51.26(4) 6_554 9_565 ?
Ni1 Dy2 Dy1 132.62(4) 13_455 9_565 ?
Dy1 Dy2 Dy1 119.20(4) . 9_565 ?
Ni1 Ge1 Ni1 131.15(13) . 2_565 ?
Ni1 Ge1 Ge1 114.43(6) . 9_566 ?
Ni1 Ge1 Ge1 114.43(6) 2_565 9_566 ?
Ni1 Ge1 Dy1 65.57(6) . . ?
Ni1 Ge1 Dy1 65.57(6) 2_565 . ?
Ge1 Ge1 Dy1 180.0 9_566 . ?
Ni1 Ge2 Ni1 121.09(14) 13 14 ?
Ni1 Ge2 Ge2 119.45(7) 13 9_665 ?
Ni1 Ge2 Ge2 119.45(7) 14 9_665 ?
Ni1 Ge2 Dy1 69.91(6) 13 . ?
Ni1 Ge2 Dy1 69.91(6) 14 . ?
Ge2 Ge2 Dy1 134.30(4) 9_665 . ?
Ni1 Ge2 Dy1 69.91(6) 13 1_655 ?
Ni1 Ge2 Dy1 69.91(6) 14 1_655 ?
Ge2 Ge2 Dy1 134.30(4) 9_665 1_655 ?
Dy1 Ge2 Dy1 91.39(8) . 1_655 ?
Ni1 Ge2 Dy2 69.88(4) 13 1_655 ?
Ni1 Ge2 Dy2 137.480(17) 14 1_655 ?
Ge2 Ge2 Dy2 66.44(4) 9_665 1_655 ?
Dy1 Ge2 Dy2 139.63(4) . 1_655 ?
Dy1 Ge2 Dy2 78.26(2) 1_655 1_655 ?
Ni1 Ge2 Dy2 69.88(4) 13 . ?
Ni1 Ge2 Dy2 137.481(17) 14 . ?
Ge2 Ge2 Dy2 66.44(4) 9_665 . ?
Dy1 Ge2 Dy2 78.26(2) . . ?
Dy1 Ge2 Dy2 139.63(4) 1_655 . ?
Dy2 Ge2 Dy2 84.83(4) 1_655 . ?
Ni1 Ge2 Dy2 137.481(18) 13 9_665 ?
Ni1 Ge2 Dy2 69.88(4) 14 9_665 ?
Ge2 Ge2 Dy2 66.44(4) 9_665 9_665 ?
Dy1 Ge2 Dy2 139.63(4) . 9_665 ?
Dy1 Ge2 Dy2 78.26(2) 1_655 9_665 ?
Dy2 Ge2 Dy2 76.74(5) 1_655 9_665 ?
Dy2 Ge2 Dy2 132.88(9) . 9_665 ?
Ni1 Ge2 Dy2 137.481(18) 13 9_565 ?
Ni1 Ge2 Dy2 69.88(4) 14 9_565 ?
Ge2 Ge2 Dy2 66.44(4) 9_665 9_565 ?
Dy1 Ge2 Dy2 78.26(2) . 9_565 ?
Dy1 Ge2 Dy2 139.63(4) 1_655 9_565 ?
Dy2 Ge2 Dy2 132.88(9) 1_655 9_565 ?
Dy2 Ge2 Dy2 76.74(5) . 9_565 ?
Dy2 Ge2 Dy2 84.83(4) 9_665 9_565 ?
Ni1 Ge3 Ni1 124.22(12) 13 13_455 ?
Ni1 Ge3 Ni1 97.73(8) 13 . ?
Ni1 Ge3 Ni1 97.73(8) 13_455 . ?
Ni1 Ge3 Ge3 113.35(6) 13 2 ?
Ni1 Ge3 Ge3 113.35(6) 13_455 2 ?
Ni1 Ge3 Ge3 105.35(7) . 2 ?
Ni1 Ge3 Dy1 159.95(8) 13 13_455 ?
Ni1 Ge3 Dy1 72.60(5) 13_455 13_455 ?
Ni1 Ge3 Dy1 67.05(5) . 13_455 ?
Ge3 Ge3 Dy1 61.77(3) 2 13_455 ?
Ni1 Ge3 Dy1 72.60(5) 13 13 ?
Ni1 Ge3 Dy1 159.95(8) 13_455 13 ?
Ni1 Ge3 Dy1 67.05(5) . 13 ?
Ge3 Ge3 Dy1 61.77(3) 2 13 ?
Dy1 Ge3 Dy1 88.95(5) 13_455 13 ?
Ni1 Ge3 Dy1 68.15(7) 13 . ?
Ni1 Ge3 Dy1 68.15(7) 13_455 . ?
Ni1 Ge3 Dy1 69.45(7) . . ?
Ge3 Ge3 Dy1 174.81(4) 2 . ?
Dy1 Ge3 Dy1 115.01(4) 13_455 . ?
Dy1 Ge3 Dy1 115.01(4) 13 . ?
Ni1 Ge3 Dy2 68.32(6) 13 . ?
Ni1 Ge3 Dy2 68.32(6) 13_455 . ?
Ni1 Ge3 Dy2 144.54(9) . . ?
Ge3 Ge3 Dy2 110.10(4) 2 . ?
Dy1 Ge3 Dy2 131.63(3) 13_455 . ?
Dy1 Ge3 Dy2 131.63(3) 13 . ?
Dy1 Ge3 Dy2 75.09(5) . . ?
Ge3 Ni1 Ge3 124.22(12) 13 13_455 ?
Ge3 Ni1 Ge2 117.86(6) 13 13 ?
Ge3 Ni1 Ge2 117.86(6) 13_455 13 ?
Ge3 Ni1 Ge3 82.27(8) 13 . ?
Ge3 Ni1 Ge3 82.27(8) 13_455 . ?
Ge2 Ni1 Ge3 104.10(11) 13 . ?
Ge3 Ni1 Ge1 75.04(7) 13 . ?
Ge3 Ni1 Ge1 75.04(7) 13_455 . ?
Ge2 Ni1 Ge1 126.12(11) 13 . ?
Ge3 Ni1 Ge1 129.78(11) . . ?
Ge3 Ni1 Dy1 143.10(10) 13 13_455 ?
Ge3 Ni1 Dy1 66.33(5) 13_455 13_455 ?
Ge2 Ni1 Dy1 63.09(6) 13 13_455 ?
Ge3 Ni1 Dy1 63.27(5) . 13_455 ?
Ge1 Ni1 Dy1 137.16(3) . 13_455 ?
Ge3 Ni1 Dy1 66.33(5) 13 13 ?
Ge3 Ni1 Dy1 143.10(10) 13_455 13 ?
Ge2 Ni1 Dy1 63.09(6) 13 13 ?
Ge3 Ni1 Dy1 63.27(5) . 13 ?
Ge1 Ni1 Dy1 137.16(3) . 13 ?
Dy1 Ni1 Dy1 85.61(6) 13_455 13 ?
Ge3 Ni1 Dy2 68.30(5) 13 13 ?
Ge3 Ni1 Dy2 141.74(9) 13_455 13 ?
Ge2 Ni1 Dy2 65.45(6) 13 13 ?
Ge3 Ni1 Dy2 135.64(4) . 13 ?
Ge1 Ni1 Dy2 74.56(5) . 13 ?
Dy1 Ni1 Dy2 128.41(8) 13_455 13 ?
Dy1 Ni1 Dy2 74.54(4) 13 13 ?
Ge3 Ni1 Dy2 141.74(9) 13 13_455 ?
Ge3 Ni1 Dy2 68.30(5) 13_455 13_455 ?
Ge2 Ni1 Dy2 65.45(6) 13 13_455 ?
Ge3 Ni1 Dy2 135.64(4) . 13_455 ?
Ge1 Ni1 Dy2 74.56(5) . 13_455 ?
Dy1 Ni1 Dy2 74.54(4) 13_455 13_455 ?
Dy1 Ni1 Dy2 128.41(8) 13 13_455 ?
Dy2 Ni1 Dy2 81.59(6) 13 13_455 ?
Ge3 Ni1 Dy1 62.65(6) 13 . ?
Ge3 Ni1 Dy1 62.65(6) 13_455 . ?
Ge2 Ni1 Dy1 166.57(10) 13 . ?
Ge3 Ni1 Dy1 62.47(7) . . ?
Ge1 Ni1 Dy1 67.31(7) . . ?
Dy1 Ni1 Dy1 107.82(6) 13_455 . ?
Dy1 Ni1 Dy1 107.82(6) 13 . ?
Dy2 Ni1 Dy1 123.45(6) 13 . ?
Dy2 Ni1 Dy1 123.45(6) 13_455 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 Ge2 2.9193(19) . ?
Dy1 Ge2 2.9193(19) 1_455 ?
Dy1 Ge3 2.9821(13) 13 ?
Dy1 Ge3 2.9821(13) 13_455 ?
Dy1 Ge3 2.9821(13) 14 ?
Dy1 Ge3 2.9821(13) 14_455 ?
Dy1 Ge3 3.0340(19) . ?
Dy1 Ge3 3.0341(19) 2_565 ?
Dy1 Ni1 3.0746(18) 13_455 ?
Dy1 Ni1 3.0746(18) 13 ?
Dy1 Ni1 3.0747(18) 14 ?
Dy1 Ni1 3.0747(18) 14_455 ?
Dy2 Ge2 3.0975(12) . ?
Dy2 Ge2 3.0975(12) 9_665 ?
Dy2 Ge2 3.0975(12) 9_565 ?
Dy2 Ge2 3.0975(12) 1_455 ?
Dy2 Ge3 3.1971(18) 10 ?
Dy2 Ge3 3.1971(18) . ?
Dy2 Ni1 3.1976(18) 6_454 ?
Dy2 Ni1 3.1976(18) 13 ?
Dy2 Ni1 3.1976(18) 6_554 ?
Dy2 Ni1 3.1976(18) 13_455 ?
Dy2 Dy1 3.7995(12) 9_565 ?
Ge1 Ni1 2.578(2) . ?
Ge1 Ni1 2.578(2) 2_565 ?
Ge1 Ge1 2.698(4) 9_566 ?
Ge2 Ni1 2.394(3) 13 ?
Ge2 Ni1 2.394(3) 14 ?
Ge2 Ge2 2.476(5) 9_665 ?
Ge2 Dy1 2.9193(19) 1_655 ?
Ge2 Dy2 3.0975(12) 1_655 ?
Ge2 Dy2 3.0975(12) 9_665 ?
Ge2 Dy2 3.0975(12) 9_565 ?
Ge3 Ni1 2.3637(14) 13 ?
Ge3 Ni1 2.3637(14) 13_455 ?
Ge3 Ni1 2.546(3) . ?
Ge3 Ge3 2.821(4) 2 ?
Ge3 Dy1 2.9821(13) 13_455 ?
Ge3 Dy1 2.9821(13) 13 ?
Ni1 Ge3 2.3637(14) 13 ?
Ni1 Ge3 2.3637(14) 13_455 ?
Ni1 Ge2 2.394(3) 13 ?
Ni1 Dy1 3.0746(18) 13_455 ?
Ni1 Dy1 3.0746(18) 13 ?
Ni1 Dy2 3.1976(18) 13 ?
Ni1 Dy2 3.1976(18) 13_455 ?
