#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:32:23 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179145 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/06/4310638.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4310638
loop_
_publ_author_name
'J. R. Salvador'
'J. R. Gour'
'D. Bilc'
'S. D. Mahanti'
'M. G. Kanatzidis'
_publ_section_title
;
 Stabilization of New Forms of the Intermetallic Phases β-RENiGe2 (RE =
 Dy, Ho, Er, Tm, Yb, Lu) in Liquid Indium
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1403
_journal_page_last               1410
_journal_paper_doi               10.1021/ic035303j
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'Er Ge2 Ni'
_chemical_formula_weight         371.15
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   4.114(2)
_cell_length_b                   8.430(5)
_cell_length_c                   15.741(9)
_cell_measurement_temperature    293(2)
_cell_volume                     545.9(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0324
_diffrn_reflns_av_sigmaI/netI    0.0182
_diffrn_reflns_limit_h_max       2
_diffrn_reflns_limit_h_min       -5
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            1845
_diffrn_reflns_theta_full        27.06
_diffrn_reflns_theta_max         27.06
_diffrn_reflns_theta_min         2.59
_exptl_absorpt_coefficient_mu    58.656
_exptl_crystal_density_diffrn    9.031
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             640
_refine_diff_density_max         2.080
_refine_diff_density_min         -1.942
_refine_diff_density_rms         0.525
_refine_ls_extinction_coef       0.0047(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.763
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     30
_refine_ls_number_reflns         378
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.763
_refine_ls_R_factor_all          0.0266
_refine_ls_R_factor_gt           0.0253
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0787P)²+80.2883P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0855
_refine_ls_wR_factor_ref         0.0871
_reflns_number_gt                362
_reflns_number_total             378
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic035303jsi20031111_122754_2.cif
_cod_data_source_block           ernige3m
_cod_original_cell_volume        546.0(5)
_cod_database_code               4310638
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Er1 Er 0.0000 0.5000 0.20395(5) 0.0048(3) Uani 1 4 d S . .
Er2 Er 0.0000 0.26022(9) 0.0000 0.0066(3) Uani 1 4 d S . .
Ge3 Ge 0.0000 0.15676(16) 0.19582(8) 0.0065(4) Uani 1 2 d S . .
Ge1 Ge 0.0000 0.5000 0.42037(13) 0.0104(5) Uani 1 4 d S . .
Ge2 Ge -0.5000 0.5000 0.07696(12) 0.0053(5) Uani 1 4 d S . .
Ni6 Ni 0.0000 0.24897(18) 0.35219(12) 0.0059(5) Uani 1 2 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Er Er -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ge2 Er1 Ge2 91.65(7) 1_655 . ?
Ge2 Er1 Ge3 88.24(2) 1_655 . ?
Ge2 Er1 Ge3 88.24(2) . . ?
Ge2 Er1 Ge3 88.24(2) 1_655 2_565 ?
Ge2 Er1 Ge3 88.24(2) . 2_565 ?
Ge3 Er1 Ge3 174.94(6) . 2_565 ?
Ge2 Er1 Ge3 82.58(5) 1_655 13 ?
Ge2 Er1 Ge3 152.24(3) . 13 ?
Ge3 Er1 Ge3 64.55(4) . 13 ?
Ge3 Er1 Ge3 118.53(3) 2_565 13 ?
Ge2 Er1 Ge3 152.24(3) 1_655 13_455 ?
Ge2 Er1 Ge3 82.58(5) . 13_455 ?
Ge3 Er1 Ge3 64.55(4) . 13_455 ?
Ge3 Er1 Ge3 118.53(3) 2_565 13_455 ?
Ge3 Er1 Ge3 89.98(5) 13 13_455 ?
Ge2 Er1 Ge3 82.58(5) 1_655 14 ?
Ge2 Er1 Ge3 152.24(3) . 14 ?
Ge3 Er1 Ge3 118.53(3) . 14 ?
Ge3 Er1 Ge3 64.55(4) 2_565 14 ?
Ge3 Er1 Ge3 54.01(6) 13 14 ?
Ge3 Er1 Ge3 114.33(6) 13_455 14 ?
Ge2 Er1 Ge3 152.24(3) 1_655 14_455 ?
Ge2 Er1 Ge3 82.58(5) . 14_455 ?
Ge3 Er1 Ge3 118.53(3) . 14_455 ?
Ge3 Er1 Ge3 64.55(4) 2_565 14_455 ?
Ge3 Er1 Ge3 114.33(6) 13 14_455 ?
Ge3 Er1 Ge3 54.01(6) 13_455 14_455 ?
Ge3 Er1 Ge3 89.98(5) 14 14_455 ?
Ge2 Er1 Ni6 106.27(5) 1_655 13_455 ?
Ge2 Er1 Ni6 47.04(4) . 13_455 ?
Ge3 Er1 Ni6 45.90(3) . 13_455 ?
Ge3 Er1 Ni6 132.11(4) 2_565 13_455 ?
Ge3 Er1 Ni6 108.63(5) 13 13_455 ?
Ge3 Er1 Ni6 51.07(5) 13_455 13_455 ?
Ge3 Er1 Ni6 160.15(5) 14 13_455 ?
Ge3 Er1 Ni6 89.59(5) 14_455 13_455 ?
Ge2 Er1 Ni6 47.04(4) 1_655 13 ?
Ge2 Er1 Ni6 106.27(5) . 13 ?
Ge3 Er1 Ni6 45.90(3) . 13 ?
Ge3 Er1 Ni6 132.11(4) 2_565 13 ?
Ge3 Er1 Ni6 51.07(5) 13 13 ?
Ge3 Er1 Ni6 108.63(5) 13_455 13 ?
Ge3 Er1 Ni6 89.59(5) 14 13 ?
Ge3 Er1 Ni6 160.15(5) 14_455 13 ?
Ni6 Er1 Ni6 84.19(6) 13_455 13 ?
Ge2 Er1 Ni6 47.04(4) 1_655 14 ?
Ge2 Er1 Ni6 106.27(5) . 14 ?
Ge3 Er1 Ni6 132.11(4) . 14 ?
Ge3 Er1 Ni6 45.90(3) 2_565 14 ?
Ge3 Er1 Ni6 89.59(5) 13 14 ?
Ge3 Er1 Ni6 160.15(5) 13_455 14 ?
Ge3 Er1 Ni6 51.07(5) 14 14 ?
Ge3 Er1 Ni6 108.63(5) 14_455 14 ?
Ni6 Er1 Ni6 146.53(7) 13_455 14 ?
Ni6 Er1 Ni6 86.30(6) 13 14 ?
Ge2 Er1 Ni6 106.27(5) 1_655 14_455 ?
Ge2 Er1 Ni6 47.04(4) . 14_455 ?
Ge3 Er1 Ni6 132.11(4) . 14_455 ?
Ge3 Er1 Ni6 45.90(3) 2_565 14_455 ?
Ge3 Er1 Ni6 160.15(5) 13 14_455 ?
Ge3 Er1 Ni6 89.59(5) 13_455 14_455 ?
Ge3 Er1 Ni6 108.63(5) 14 14_455 ?
Ge3 Er1 Ni6 51.07(5) 14_455 14_455 ?
Ni6 Er1 Ni6 86.30(6) 13_455 14_455 ?
Ni6 Er1 Ni6 146.53(7) 13 14_455 ?
Ni6 Er1 Ni6 84.19(6) 14 14_455 ?
Ni6 Er2 Ni6 177.14(6) 6_454 13 ?
Ni6 Er2 Ni6 82.93(6) 6_454 6_554 ?
Ni6 Er2 Ni6 97.00(6) 13 6_554 ?
Ni6 Er2 Ni6 97.00(6) 6_454 13_455 ?
Ni6 Er2 Ni6 82.93(6) 13 13_455 ?
Ni6 Er2 Ni6 177.14(6) 6_554 13_455 ?
Ni6 Er2 Ge2 82.57(5) 6_454 . ?
Ni6 Er2 Ge2 99.30(5) 13 . ?
Ni6 Er2 Ge2 137.87(5) 6_554 . ?
Ni6 Er2 Ge2 44.81(4) 13_455 . ?
Ni6 Er2 Ge2 137.87(5) 6_454 1_655 ?
Ni6 Er2 Ge2 44.81(4) 13 1_655 ?
Ni6 Er2 Ge2 82.57(5) 6_554 1_655 ?
Ni6 Er2 Ge2 99.29(5) 13_455 1_655 ?
Ge2 Er2 Ge2 82.24(5) . 1_655 ?
Ni6 Er2 Ge2 99.29(5) 6_454 9_565 ?
Ni6 Er2 Ge2 82.57(5) 13 9_565 ?
Ni6 Er2 Ge2 44.81(4) 6_554 9_565 ?
Ni6 Er2 Ge2 137.87(5) 13_455 9_565 ?
Ge2 Er2 Ge2 99.50(5) . 9_565 ?
Ge2 Er2 Ge2 45.57(7) 1_655 9_565 ?
Ni6 Er2 Ge2 44.81(4) 6_454 9_465 ?
Ni6 Er2 Ge2 137.87(5) 13 9_465 ?
Ni6 Er2 Ge2 99.29(5) 6_554 9_465 ?
Ni6 Er2 Ge2 82.57(5) 13_455 9_465 ?
Ge2 Er2 Ge2 45.57(7) . 9_465 ?
Ge2 Er2 Ge2 99.49(5) 1_655 9_465 ?
Ge2 Er2 Ge2 82.24(5) 9_565 9_465 ?
Ni6 Er2 Ge3 135.55(4) 6_454 . ?
Ni6 Er2 Ge3 43.33(3) 13 . ?
Ni6 Er2 Ge3 135.55(3) 6_554 . ?
Ni6 Er2 Ge3 43.33(3) 13_455 . ?
Ge2 Er2 Ge3 78.65(4) . . ?
Ge2 Er2 Ge3 78.65(4) 1_655 . ?
Ge2 Er2 Ge3 123.27(4) 9_565 . ?
Ge2 Er2 Ge3 123.27(4) 9_465 . ?
Ni6 Er2 Ge3 43.33(3) 6_454 10 ?
Ni6 Er2 Ge3 135.55(3) 13 10 ?
Ni6 Er2 Ge3 43.33(3) 6_554 10 ?
Ni6 Er2 Ge3 135.55(4) 13_455 10 ?
Ge2 Er2 Ge3 123.27(4) . 10 ?
Ge2 Er2 Ge3 123.27(4) 1_655 10 ?
Ge2 Er2 Ge3 78.65(4) 9_565 10 ?
Ge2 Er2 Ge3 78.65(4) 9_465 10 ?
Ge3 Er2 Ge3 148.40(6) . 10 ?
Ni6 Er2 Ge1 43.69(4) 6_454 5_444 ?
Ni6 Er2 Ge1 133.59(5) 13 5_444 ?
Ni6 Er2 Ge1 96.50(5) 6_554 5_444 ?
Ni6 Er2 Ge1 81.56(5) 13_455 5_444 ?
Ge2 Er2 Ge1 99.72(4) . 5_444 ?
Ge2 Er2 Ge1 177.83(2) 1_655 5_444 ?
Ge2 Er2 Ge1 134.53(6) 9_565 5_444 ?
Ge2 Er2 Ge1 82.58(4) 9_465 5_444 ?
Ge3 Er2 Ge1 100.77(5) . 5_444 ?
Ge3 Er2 Ge1 56.39(4) 10 5_444 ?
Ni6 Er2 Ge1 81.56(5) 6_454 13_455 ?
Ni6 Er2 Ge1 96.50(5) 13 13_455 ?
Ni6 Er2 Ge1 133.59(5) 6_554 13_455 ?
Ni6 Er2 Ge1 43.69(4) 13_455 13_455 ?
Ge2 Er2 Ge1 82.58(4) . 13_455 ?
Ge2 Er2 Ge1 134.53(6) 1_655 13_455 ?
Ge2 Er2 Ge1 177.83(2) 9_565 13_455 ?
Ge2 Er2 Ge1 99.72(4) 9_465 13_455 ?
Ge3 Er2 Ge1 56.39(4) . 13_455 ?
Ge3 Er2 Ge1 100.77(5) 10 13_455 ?
Ge1 Er2 Ge1 45.26(7) 5_444 13_455 ?
Ni6 Ge3 Ni6 123.88(10) 13 13_455 ?
Ni6 Ge3 Ni6 101.92(6) 13 . ?
Ni6 Ge3 Ni6 101.92(6) 13_455 . ?
Ni6 Ge3 Ge3 109.93(5) 13 2 ?
Ni6 Ge3 Ge3 109.93(5) 13_455 2 ?
Ni6 Ge3 Ge3 107.53(5) . 2 ?
Ni6 Ge3 Er1 70.96(5) 13 . ?
Ni6 Ge3 Er1 70.96(5) 13_455 . ?
Ni6 Ge3 Er1 69.94(5) . . ?
Ge3 Ge3 Er1 177.47(3) 2 . ?
Ni6 Ge3 Er1 72.95(5) 13 13 ?
Ni6 Ge3 Er1 162.64(6) 13_455 13 ?
Ni6 Ge3 Er1 67.65(4) . 13 ?
Ge3 Ge3 Er1 62.99(3) 2 13 ?
Er1 Ge3 Er1 115.45(4) . 13 ?
Ni6 Ge3 Er1 162.64(6) 13 13_455 ?
Ni6 Ge3 Er1 72.95(5) 13_455 13_455 ?
Ni6 Ge3 Er1 67.65(4) . 13_455 ?
Ge3 Ge3 Er1 62.99(3) 2 13_455 ?
Er1 Ge3 Er1 115.45(4) . 13_455 ?
Er1 Ge3 Er1 89.98(5) 13 13_455 ?
Ni6 Ge3 Er2 66.13(5) 13 . ?
Ni6 Ge3 Er2 66.13(5) 13_455 . ?
Ni6 Ge3 Er2 146.68(7) . . ?
Ge3 Ge3 Er2 105.80(3) 2 . ?
Er1 Ge3 Er2 76.73(4) . . ?
Er1 Ge3 Er2 130.19(3) 13 . ?
Er1 Ge3 Er2 130.19(3) 13_455 . ?
Ni6 Ge1 Ni6 126.21(12) . 2_565 ?
Ni6 Ge1 Ge1 116.89(6) . 9_566 ?
Ni6 Ge1 Ge1 116.89(6) 2_565 9_566 ?
Ni6 Ge1 Er2 64.76(4) . 13_455 ?
Ni6 Ge1 Er2 140.76(2) 2_565 13_455 ?
Ge1 Ge1 Er2 67.37(4) 9_566 13_455 ?
Ni6 Ge1 Er2 64.76(4) . 13 ?
Ni6 Ge1 Er2 140.76(2) 2_565 13 ?
Ge1 Ge1 Er2 67.37(4) 9_566 13 ?
Er2 Ge1 Er2 78.31(5) 13_455 13 ?
Ni6 Ge1 Er2 140.76(2) . 5 ?
Ni6 Ge1 Er2 64.76(4) 2_565 5 ?
Ge1 Ge1 Er2 67.37(4) 9_566 5 ?
Er2 Ge1 Er2 134.74(7) 13_455 5 ?
Er2 Ge1 Er2 84.64(5) 13 5 ?
Ni6 Ge1 Er2 140.76(2) . 5_455 ?
Ni6 Ge1 Er2 64.76(4) 2_565 5_455 ?
Ge1 Ge1 Er2 67.37(4) 9_566 5_455 ?
Er2 Ge1 Er2 84.64(5) 13_455 5_455 ?
Er2 Ge1 Er2 134.74(7) 13 5_455 ?
Er2 Ge1 Er2 78.31(5) 5 5_455 ?
Ni6 Ge1 Er1 63.11(6) . . ?
Ni6 Ge1 Er1 63.11(6) 2_565 . ?
Ge1 Ge1 Er1 180.0 9_566 . ?
Er2 Ge1 Er1 112.63(4) 13_455 . ?
Er2 Ge1 Er1 112.63(4) 13 . ?
Er2 Ge1 Er1 112.63(4) 5 . ?
Er2 Ge1 Er1 112.63(4) 5_455 . ?
Ni6 Ge2 Ni6 124.03(12) 13_455 14_455 ?
Ni6 Ge2 Ge2 117.99(6) 13_455 9_465 ?
Ni6 Ge2 Ge2 117.99(6) 14_455 9_465 ?
Ni6 Ge2 Er1 70.91(5) 13_455 . ?
Ni6 Ge2 Er1 70.91(5) 14_455 . ?
Ge2 Ge2 Er1 134.18(4) 9_465 . ?
Ni6 Ge2 Er1 70.91(5) 13_455 1_455 ?
Ni6 Ge2 Er1 70.91(5) 14_455 1_455 ?
Ge2 Ge2 Er1 134.18(4) 9_465 1_455 ?
Er1 Ge2 Er1 91.65(7) . 1_455 ?
Ni6 Ge2 Er2 67.12(4) 13_455 1_455 ?
Ni6 Ge2 Er2 138.79(2) 14_455 1_455 ?
Ge2 Ge2 Er2 67.21(3) 9_465 1_455 ?
Er1 Ge2 Er2 137.86(4) . 1_455 ?
Er1 Ge2 Er2 78.36(3) 1_455 1_455 ?
Ni6 Ge2 Er2 138.79(2) 13_455 9_565 ?
Ni6 Ge2 Er2 67.12(4) 14_455 9_565 ?
Ge2 Ge2 Er2 67.21(3) 9_465 9_565 ?
Er1 Ge2 Er2 78.36(3) . 9_565 ?
Er1 Ge2 Er2 137.86(4) 1_455 9_565 ?
Er2 Ge2 Er2 134.43(7) 1_455 9_565 ?
Ni6 Ge2 Er2 67.12(4) 13_455 . ?
Ni6 Ge2 Er2 138.79(2) 14_455 . ?
Ge2 Ge2 Er2 67.21(3) 9_465 . ?
Er1 Ge2 Er2 78.36(3) . . ?
Er1 Ge2 Er2 137.86(4) 1_455 . ?
Er2 Ge2 Er2 82.24(5) 1_455 . ?
Er2 Ge2 Er2 80.50(5) 9_565 . ?
Ni6 Ge2 Er2 138.79(2) 13_455 9_465 ?
Ni6 Ge2 Er2 67.12(4) 14_455 9_465 ?
Ge2 Ge2 Er2 67.21(3) 9_465 9_465 ?
Er1 Ge2 Er2 137.86(4) . 9_465 ?
Er1 Ge2 Er2 78.36(3) 1_455 9_465 ?
Er2 Ge2 Er2 80.50(5) 1_455 9_465 ?
Er2 Ge2 Er2 82.24(5) 9_565 9_465 ?
Er2 Ge2 Er2 134.43(7) . 9_465 ?
Ge3 Ni6 Ge3 123.87(10) 13 13_455 ?
Ge3 Ni6 Ge1 80.94(6) 13 . ?
Ge3 Ni6 Ge1 80.94(6) 13_455 . ?
Ge3 Ni6 Ge2 116.95(5) 13 13_455 ?
Ge3 Ni6 Ge2 116.95(5) 13_455 13_455 ?
Ge1 Ni6 Ge2 125.12(10) . 13_455 ?
Ge3 Ni6 Ge3 78.08(6) 13 . ?
Ge3 Ni6 Ge3 78.08(6) 13_455 . ?
Ge1 Ni6 Ge3 134.42(9) . . ?
Ge2 Ni6 Ge3 100.46(8) 13_455 . ?
Ge3 Ni6 Er1 137.00(8) 13 13_455 ?
Ge3 Ni6 Er1 63.14(5) 13_455 13_455 ?
Ge1 Ni6 Er1 137.75(3) . 13_455 ?
Ge2 Ni6 Er1 62.04(5) 13_455 13_455 ?
Ge3 Ni6 Er1 61.28(4) . 13_455 ?
Ge3 Ni6 Er1 63.14(5) 13 13 ?
Ge3 Ni6 Er1 137.00(8) 13_455 13 ?
Ge1 Ni6 Er1 137.75(3) . 13 ?
Ge2 Ni6 Er1 62.04(5) 13_455 13 ?
Ge3 Ni6 Er1 61.28(4) . 13 ?
Er1 Ni6 Er1 84.19(6) 13_455 13 ?
Ge3 Ni6 Er2 70.55(5) 13 13 ?
Ge3 Ni6 Er2 146.68(7) 13_455 13 ?
Ge1 Ni6 Er2 71.55(5) . 13 ?
Ge2 Ni6 Er2 68.07(5) 13_455 13 ?
Ge3 Ni6 Er2 134.96(4) . 13 ?
Er1 Ni6 Er2 129.98(6) 13_455 13 ?
Er1 Ni6 Er2 75.80(4) 13 13 ?
Ge3 Ni6 Er2 146.68(7) 13 13_455 ?
Ge3 Ni6 Er2 70.55(5) 13_455 13_455 ?
Ge1 Ni6 Er2 71.55(5) . 13_455 ?
Ge2 Ni6 Er2 68.07(5) 13_455 13_455 ?
Ge3 Ni6 Er2 134.96(4) . 13_455 ?
Er1 Ni6 Er2 75.80(4) 13_455 13_455 ?
Er1 Ni6 Er2 129.98(6) 13 13_455 ?
Er2 Ni6 Er2 82.93(6) 13 13_455 ?
Ge3 Ni6 Er1 62.02(5) 13 . ?
Ge3 Ni6 Er1 62.02(5) 13_455 . ?
Ge1 Ni6 Er1 74.69(7) . . ?
Ge2 Ni6 Er1 160.19(8) 13_455 . ?
Ge3 Ni6 Er1 59.73(6) . . ?
Er1 Ni6 Er1 104.25(5) 13_455 . ?
Er1 Ni6 Er1 104.25(5) 13 . ?
Er2 Ni6 Er1 124.86(4) 13 . ?
Er2 Ni6 Er1 124.86(4) 13_455 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Er1 Ge2 2.8684(18) 1_655 ?
Er1 Ge2 2.8684(18) . ?
Er1 Ge3 2.896(2) . ?
Er1 Ge3 2.896(2) 2_565 ?
Er1 Ge3 2.9099(14) 13 ?
Er1 Ge3 2.9099(14) 13_455 ?
Er1 Ge3 2.9099(14) 14 ?
Er1 Ge3 2.9099(14) 14_455 ?
Er1 Ni6 3.0688(16) 13_455 ?
Er1 Ni6 3.0688(16) 13 ?
Er1 Ni6 3.0688(16) 14 ?
Er1 Ni6 3.0688(16) 14_455 ?
Er2 Ni6 3.1068(18) 6_454 ?
Er2 Ni6 3.1068(18) 13 ?
Er2 Ni6 3.1068(18) 6_554 ?
Er2 Ni6 3.1068(18) 13_455 ?
Er2 Ge2 3.1282(13) . ?
Er2 Ge2 3.1282(13) 1_655 ?
Er2 Ge2 3.1282(13) 9_565 ?
Er2 Ge2 3.1282(13) 9_465 ?
Er2 Ge3 3.204(2) . ?
Er2 Ge3 3.204(2) 10 ?
Er2 Ge1 3.2581(14) 5_444 ?
Er2 Ge1 3.2581(14) 13_455 ?
Ge3 Ni6 2.3313(14) 13 ?
Ge3 Ni6 2.3313(14) 13_455 ?
Ge3 Ni6 2.581(3) . ?
Ge3 Ge3 2.643(3) 2 ?
Ge3 Er1 2.9099(14) 13 ?
Ge3 Er1 2.9099(14) 13_455 ?
Ge1 Ni6 2.373(2) . ?
Ge1 Ni6 2.373(2) 2_565 ?
Ge1 Ge1 2.507(4) 9_566 ?
Ge1 Er2 3.2581(14) 13_455 ?
Ge1 Er2 3.2581(14) 13 ?
Ge1 Er2 3.2581(14) 5 ?
Ge1 Er2 3.2581(14) 5_455 ?
Ge2 Ni6 2.377(2) 13_455 ?
Ge2 Ni6 2.377(2) 14_455 ?
Ge2 Ge2 2.423(4) 9_465 ?
Ge2 Er1 2.8684(18) 1_455 ?
Ge2 Er2 3.1281(13) 1_455 ?
Ge2 Er2 3.1282(13) 9_565 ?
Ge2 Er2 3.1282(13) 9_465 ?
Ni6 Ge3 2.3313(14) 13 ?
Ni6 Ge3 2.3313(14) 13_455 ?
Ni6 Ge2 2.377(2) 13_455 ?
Ni6 Er1 3.0688(16) 13_455 ?
Ni6 Er1 3.0688(16) 13 ?
Ni6 Er2 3.1067(18) 13 ?
Ni6 Er2 3.1067(18) 13_455 ?
