#------------------------------------------------------------------------------
#$Date: 2016-03-23 01:40:27 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179150 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/11/4311170.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4311170
loop_
_publ_author_name
'Richard D. Adams'
'Burjor Captain'
'Wei Fu'
'Michael B. Hall'
'Mark D. Smith'
'Charles Edwin Webster'
_publ_section_title
;
 Dinuclear Ruthenium and Iron Complexes Containing Palladium and Platinum
 with Tri-tert-Butylphosphine Ligands: Synthesis, Structures, and Bonding
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3921
_journal_page_last               3929
_journal_paper_doi               10.1021/ic049675j
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'C33 H54 O9 P2 Pt2 Ru2'
_chemical_formula_weight         1249.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.2620(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.5394(10)
_cell_length_b                   16.2556(11)
_cell_length_c                   17.0963(12)
_cell_measurement_reflns_used    6949
_cell_measurement_temperature    190(2)
_cell_measurement_theta_max      25.02
_cell_measurement_theta_min      2.22
_cell_volume                     4040.6(5)
_computing_cell_refinement       'SAINT+ NT V6.02a (Bruker, 1998)'
_computing_data_collection       'SMART NT V5.619 (Bruker, 2000)'
_computing_data_reduction        'SAINT+ NT V6.02a'
_computing_molecular_graphics    'SHELXTL V5.1 (Sheldrick, 1997)'
_computing_publication_material  'SHELXTL V5.1'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      190(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker SMART APEX CCD diffractometer'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0350
_diffrn_reflns_av_sigmaI/netI    0.0347
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            23803
_diffrn_reflns_theta_full        25.03
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_min         1.73
_diffrn_standards_decay_%        <1
_exptl_absorpt_coefficient_mu    7.762
_exptl_absorpt_correction_T_max  0.4146
_exptl_absorpt_correction_T_min  0.2924
_exptl_absorpt_correction_type   SADABS
_exptl_absorpt_process_details   '(SADABS, Bruker, 1997)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.053
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             2392
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.38
_exptl_crystal_size_min          0.24
_refine_diff_density_max         1.021
_refine_diff_density_min         -0.720
_refine_diff_density_rms         0.153
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.984
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         7132
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.984
_refine_ls_R_factor_all          0.0309
_refine_ls_R_factor_gt           0.0254
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0283P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0563
_refine_ls_wR_factor_ref         0.0577
_reflns_number_gt                6140
_reflns_number_total             7132
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic049675jsi20040315_094035.cif
_cod_data_source_block           bc3542s
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4311170
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.240507(13) 0.406787(12) 0.751517(11) 0.02110(6) Uani 1 1 d . . .
Pt2 Pt 0.245482(13) 0.400434(11) 1.024848(11) 0.02024(6) Uani 1 1 d . . .
Ru1 Ru 0.31786(3) 0.46338(2) 0.88416(2) 0.02040(10) Uani 1 1 d . . .
Ru2 Ru 0.20045(3) 0.31380(2) 0.88911(2) 0.01924(9) Uani 1 1 d . . .
P1 P 0.22589(9) 0.39300(8) 0.61700(7) 0.0212(3) Uani 1 1 d . . .
P2 P 0.23228(9) 0.41589(8) 1.15892(7) 0.0205(3) Uani 1 1 d . . .
C11 C 0.3357(4) 0.5152(4) 0.7811(3) 0.0318(13) Uani 1 1 d . . .
C12 C 0.4183(4) 0.3847(3) 0.8731(3) 0.0298(13) Uani 1 1 d . . .
C13 C 0.2096(4) 0.5309(3) 0.8973(3) 0.0303(13) Uani 1 1 d . . .
C14 C 0.3873(3) 0.5289(3) 0.9559(3) 0.0247(11) Uani 1 1 d . . .
C21 C 0.1228(4) 0.3688(3) 0.7945(3) 0.0287(12) Uani 1 1 d . . .
C22 C 0.2830(3) 0.2518(3) 0.8229(3) 0.0261(12) Uani 1 1 d . . .
C23 C 0.1213(4) 0.3818(3) 0.9637(3) 0.0265(12) Uani 1 1 d . . .
C24 C 0.1147(4) 0.2271(3) 0.8958(3) 0.0286(12) Uani 1 1 d . . .
C25 C 0.2812(3) 0.2873(3) 0.9837(3) 0.0237(11) Uani 1 1 d . . .
C31 C 0.3451(4) 0.3709(4) 0.5747(3) 0.0337(13) Uani 1 1 d . . .
C32 C 0.4176(4) 0.4235(4) 0.6177(3) 0.0427(16) Uani 1 1 d . . .
H32A H 0.4787 0.4115 0.5965 0.064 Uiso 1 1 calc R . .
H32B H 0.4167 0.4105 0.6736 0.064 Uiso 1 1 calc R . .
H32C H 0.4035 0.4819 0.6102 0.064 Uiso 1 1 calc R . .
C33 C 0.3547(4) 0.3854(4) 0.4872(3) 0.0413(15) Uani 1 1 d . . .
H33A H 0.3454 0.4439 0.4758 0.062 Uiso 1 1 calc R . .
H33B H 0.3084 0.3528 0.4591 0.062 Uiso 1 1 calc R . .
H33C H 0.4163 0.3688 0.4704 0.062 Uiso 1 1 calc R . .
C34 C 0.3727(4) 0.2809(4) 0.5918(3) 0.0475(17) Uani 1 1 d . . .
H34A H 0.3342 0.2437 0.5606 0.071 Uiso 1 1 calc R . .
H34B H 0.3640 0.2692 0.6475 0.071 Uiso 1 1 calc R . .
H34C H 0.4375 0.2726 0.5782 0.071 Uiso 1 1 calc R . .
C41 C 0.1802(3) 0.4918(3) 0.5712(3) 0.0262(12) Uani 1 1 d . . .
C42 C 0.1022(4) 0.5240(3) 0.6239(3) 0.0366(14) Uani 1 1 d . . .
H42A H 0.0792 0.5764 0.6033 0.055 Uiso 1 1 calc R . .
H42B H 0.1258 0.5323 0.6771 0.055 Uiso 1 1 calc R . .
H42C H 0.0520 0.4838 0.6249 0.055 Uiso 1 1 calc R . .
C43 C 0.2541(4) 0.5581(3) 0.5737(3) 0.0350(14) Uani 1 1 d . . .
H43A H 0.3045 0.5429 0.5387 0.053 Uiso 1 1 calc R . .
H43B H 0.2776 0.5634 0.6273 0.053 Uiso 1 1 calc R . .
H43C H 0.2276 0.6107 0.5569 0.053 Uiso 1 1 calc R . .
C44 C 0.1457(4) 0.4858(3) 0.4870(3) 0.0327(13) Uani 1 1 d . . .
H44A H 0.1233 0.5397 0.4698 0.049 Uiso 1 1 calc R . .
H44B H 0.0954 0.4457 0.4841 0.049 Uiso 1 1 calc R . .
H44C H 0.1961 0.4680 0.4531 0.049 Uiso 1 1 calc R . .
C51 C 0.1464(4) 0.3059(3) 0.5850(3) 0.0290(12) Uani 1 1 d . . .
C52 C 0.1605(4) 0.2319(3) 0.6397(3) 0.0387(14) Uani 1 1 d . . .
H52A H 0.1213 0.1863 0.6224 0.058 Uiso 1 1 calc R . .
H52B H 0.1440 0.2475 0.6932 0.058 Uiso 1 1 calc R . .
H52C H 0.2251 0.2148 0.6384 0.058 Uiso 1 1 calc R . .
C53 C 0.0443(4) 0.3304(4) 0.5947(3) 0.0402(15) Uani 1 1 d . . .
H53A H 0.0286 0.3735 0.5568 0.060 Uiso 1 1 calc R . .
H53B H 0.0343 0.3511 0.6479 0.060 Uiso 1 1 calc R . .
H53C H 0.0052 0.2823 0.5856 0.060 Uiso 1 1 calc R . .
C54 C 0.1580(5) 0.2757(4) 0.5011(3) 0.0449(16) Uani 1 1 d . . .
H54A H 0.2202 0.2535 0.4945 0.067 Uiso 1 1 calc R . .
H54B H 0.1487 0.3217 0.4648 0.067 Uiso 1 1 calc R . .
H54C H 0.1127 0.2326 0.4901 0.067 Uiso 1 1 calc R . .
C61 C 0.2063(3) 0.5290(3) 1.1796(3) 0.0274(12) Uani 1 1 d . . .
C62 C 0.1715(4) 0.5481(3) 1.2628(3) 0.0355(13) Uani 1 1 d . . .
H62A H 0.1587 0.6070 1.2674 0.053 Uiso 1 1 calc R . .
H62B H 0.2187 0.5324 1.3012 0.053 Uiso 1 1 calc R . .
H62C H 0.1151 0.5168 1.2727 0.053 Uiso 1 1 calc R . .
C63 C 0.2916(4) 0.5816(3) 1.1651(3) 0.0375(14) Uani 1 1 d . . .
H63A H 0.3181 0.5673 1.1143 0.056 Uiso 1 1 calc R . .
H63B H 0.3370 0.5715 1.2065 0.056 Uiso 1 1 calc R . .
H63C H 0.2743 0.6399 1.1652 0.056 Uiso 1 1 calc R . .
C64 C 0.1348(4) 0.5579(3) 1.1198(3) 0.0369(14) Uani 1 1 d . . .
H64A H 0.0783 0.5256 1.1258 0.055 Uiso 1 1 calc R . .
H64B H 0.1589 0.5502 1.0668 0.055 Uiso 1 1 calc R . .
H64C H 0.1213 0.6162 1.1283 0.055 Uiso 1 1 calc R . .
C71 C 0.3473(4) 0.3881(3) 1.2059(3) 0.0286(12) Uani 1 1 d . . .
C72 C 0.3587(4) 0.2943(3) 1.2114(3) 0.0402(15) Uani 1 1 d . . .
H72A H 0.4205 0.2813 1.2310 0.060 Uiso 1 1 calc R . .
H72B H 0.3503 0.2698 1.1595 0.060 Uiso 1 1 calc R . .
H72C H 0.3127 0.2719 1.2473 0.060 Uiso 1 1 calc R . .
C73 C 0.3638(4) 0.4245(4) 1.2871(3) 0.0360(14) Uani 1 1 d . . .
H73A H 0.4244 0.4073 1.3064 0.054 Uiso 1 1 calc R . .
H73B H 0.3162 0.4047 1.3229 0.054 Uiso 1 1 calc R . .
H73C H 0.3613 0.4846 1.2841 0.054 Uiso 1 1 calc R . .
C74 C 0.4235(3) 0.4167(3) 1.1507(3) 0.0339(13) Uani 1 1 d . . .
H74A H 0.4208 0.4767 1.1451 0.051 Uiso 1 1 calc R . .
H74B H 0.4152 0.3909 1.0994 0.051 Uiso 1 1 calc R . .
H74C H 0.4835 0.4010 1.1724 0.051 Uiso 1 1 calc R . .
C81 C 0.1373(3) 0.3493(3) 1.2033(3) 0.0291(12) Uani 1 1 d . . .
C82 C 0.1408(4) 0.2637(3) 1.1653(3) 0.0384(14) Uani 1 1 d . . .
H82A H 0.1994 0.2372 1.1783 0.058 Uiso 1 1 calc R . .
H82B H 0.1352 0.2693 1.1084 0.058 Uiso 1 1 calc R . .
H82C H 0.0899 0.2301 1.1850 0.058 Uiso 1 1 calc R . .
C83 C 0.1430(4) 0.3396(4) 1.2919(3) 0.0383(14) Uani 1 1 d . . .
H83A H 0.1388 0.3939 1.3167 0.057 Uiso 1 1 calc R . .
H83B H 0.2017 0.3139 1.3061 0.057 Uiso 1 1 calc R . .
H83C H 0.0922 0.3049 1.3099 0.057 Uiso 1 1 calc R . .
C84 C 0.0427(4) 0.3849(4) 1.1828(3) 0.0372(14) Uani 1 1 d . . .
H84A H -0.0053 0.3472 1.2008 0.056 Uiso 1 1 calc R . .
H84B H 0.0377 0.3919 1.1261 0.056 Uiso 1 1 calc R . .
H84C H 0.0353 0.4383 1.2086 0.056 Uiso 1 1 calc R . .
O11 O 0.3619(3) 0.5695(2) 0.7439(2) 0.0458(11) Uani 1 1 d . . .
O12 O 0.4768(3) 0.3395(3) 0.8654(3) 0.0483(11) Uani 1 1 d . . .
O13 O 0.1471(3) 0.5725(2) 0.9037(3) 0.0450(11) Uani 1 1 d . . .
O14 O 0.4291(2) 0.5711(2) 0.9953(2) 0.0308(9) Uani 1 1 d . . .
O21 O 0.0460(2) 0.3834(3) 0.7821(2) 0.0498(12) Uani 1 1 d . . .
O22 O 0.3319(3) 0.2108(2) 0.7879(2) 0.0367(9) Uani 1 1 d . . .
O23 O 0.0511(2) 0.4110(2) 0.9809(2) 0.0378(10) Uani 1 1 d . . .
O24 O 0.0611(3) 0.1762(3) 0.9000(3) 0.0501(11) Uani 1 1 d . . .
O25 O 0.3336(3) 0.2417(2) 1.0119(2) 0.0410(10) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C21 Pt1 C11 133.2(2) . . ?
C21 Pt1 P1 105.34(15) . . ?
C11 Pt1 P1 110.18(14) . . ?
C21 Pt1 Ru1 98.84(15) . . ?
C11 Pt1 Ru1 45.75(13) . . ?
P1 Pt1 Ru1 154.86(3) . . ?
C21 Pt1 Ru2 49.08(15) . . ?
C11 Pt1 Ru2 110.46(13) . . ?
P1 Pt1 Ru2 138.32(3) . . ?
Ru1 Pt1 Ru2 64.715(13) . . ?
C25 Pt2 C23 85.3(2) . . ?
C25 Pt2 P2 117.55(14) . . ?
C23 Pt2 P2 115.63(15) . . ?
C25 Pt2 Ru2 46.85(14) . . ?
C23 Pt2 Ru2 46.90(15) . . ?
P2 Pt2 Ru2 149.12(3) . . ?
C25 Pt2 Ru1 86.35(14) . . ?
C23 Pt2 Ru1 87.21(14) . . ?
P2 Pt2 Ru1 146.89(3) . . ?
Ru2 Pt2 Ru1 63.964(13) . . ?
C14 Ru1 C13 92.1(2) . . ?
C14 Ru1 C12 92.0(2) . . ?
C13 Ru1 C12 173.6(2) . . ?
C14 Ru1 C11 105.4(2) . . ?
C13 Ru1 C11 88.4(2) . . ?
C12 Ru1 C11 95.3(2) . . ?
C14 Ru1 Pt1 161.88(14) . . ?
C13 Ru1 Pt1 87.40(15) . . ?
C12 Ru1 Pt1 90.22(15) . . ?
C11 Ru1 Pt1 56.52(16) . . ?
C14 Ru1 Pt2 81.52(14) . . ?
C13 Ru1 Pt2 78.46(16) . . ?
C12 Ru1 Pt2 97.30(16) . . ?
C11 Ru1 Pt2 165.45(16) . . ?
Pt1 Ru1 Pt2 116.015(15) . . ?
C14 Ru1 Ru2 137.71(14) . . ?
C13 Ru1 Ru2 89.61(16) . . ?
C12 Ru1 Ru2 84.05(15) . . ?
C11 Ru1 Ru2 116.91(16) . . ?
Pt1 Ru1 Ru2 60.402(12) . . ?
Pt2 Ru1 Ru2 57.495(11) . . ?
C24 Ru2 C22 93.3(2) . . ?
C24 Ru2 C25 99.9(2) . . ?
C22 Ru2 C25 89.88(19) . . ?
C24 Ru2 C23 89.5(2) . . ?
C22 Ru2 C23 175.9(2) . . ?
C25 Ru2 C23 86.76(19) . . ?
C24 Ru2 C21 90.7(2) . . ?
C22 Ru2 C21 95.77(19) . . ?
C25 Ru2 C21 167.7(2) . . ?
C23 Ru2 C21 87.1(2) . . ?
C24 Ru2 Pt2 118.64(16) . . ?
C22 Ru2 Pt2 127.28(14) . . ?
C25 Ru2 Pt2 46.78(14) . . ?
C23 Ru2 Pt2 48.66(14) . . ?
C21 Ru2 Pt2 122.22(15) . . ?
C24 Ru2 Pt1 125.63(16) . . ?
C22 Ru2 Pt1 70.43(14) . . ?
C25 Ru2 Pt1 130.19(14) . . ?
C23 Ru2 Pt1 110.15(14) . . ?
C21 Ru2 Pt1 43.37(13) . . ?
Pt2 Ru2 Pt1 111.694(15) . . ?
C24 Ru2 Ru1 173.29(15) . . ?
C22 Ru2 Ru1 92.98(15) . . ?
C25 Ru2 Ru1 82.34(14) . . ?
C23 Ru2 Ru1 84.29(14) . . ?
C21 Ru2 Ru1 86.45(14) . . ?
Pt2 Ru2 Ru1 58.540(11) . . ?
Pt1 Ru2 Ru1 54.883(11) . . ?
C41 P1 C51 107.4(2) . . ?
C41 P1 C31 108.5(2) . . ?
C51 P1 C31 107.6(2) . . ?
C41 P1 Pt1 110.89(16) . . ?
C51 P1 Pt1 114.12(17) . . ?
C31 P1 Pt1 108.25(17) . . ?
C71 P2 C61 108.9(2) . . ?
C71 P2 C81 109.4(2) . . ?
C61 P2 C81 109.1(2) . . ?
C71 P2 Pt2 108.35(16) . . ?
C61 P2 Pt2 107.75(16) . . ?
C81 P2 Pt2 113.21(17) . . ?
O11 C11 Ru1 149.8(4) . . ?
O11 C11 Pt1 131.8(4) . . ?
Ru1 C11 Pt1 77.7(2) . . ?
O12 C12 Ru1 178.8(5) . . ?
O13 C13 Ru1 177.9(5) . . ?
O14 C14 Ru1 176.1(4) . . ?
O21 C21 Pt1 135.0(4) . . ?
O21 C21 Ru2 136.1(4) . . ?
Pt1 C21 Ru2 87.6(2) . . ?
O22 C22 Ru2 175.0(4) . . ?
O23 C23 Ru2 150.9(4) . . ?
O23 C23 Pt2 124.6(4) . . ?
Ru2 C23 Pt2 84.4(2) . . ?
O24 C24 Ru2 178.3(5) . . ?
O25 C25 Pt2 126.7(4) . . ?
O25 C25 Ru2 146.6(4) . . ?
Pt2 C25 Ru2 86.37(19) . . ?
C33 C31 C32 108.5(5) . . ?
C33 C31 C34 107.9(5) . . ?
C32 C31 C34 105.0(5) . . ?
C33 C31 P1 115.4(4) . . ?
C32 C31 P1 109.6(4) . . ?
C34 C31 P1 109.9(4) . . ?
C43 C41 C44 107.6(4) . . ?
C43 C41 C42 105.3(4) . . ?
C44 C41 C42 109.5(4) . . ?
C43 C41 P1 109.9(3) . . ?
C44 C41 P1 116.5(4) . . ?
C42 C41 P1 107.5(4) . . ?
C54 C51 C52 107.8(4) . . ?
C54 C51 C53 107.1(5) . . ?
C52 C51 C53 105.2(4) . . ?
C54 C51 P1 116.0(4) . . ?
C52 C51 P1 109.1(4) . . ?
C53 C51 P1 111.1(4) . . ?
C63 C61 C64 105.6(5) . . ?
C63 C61 C62 107.9(4) . . ?
C64 C61 C62 109.3(4) . . ?
C63 C61 P2 110.4(3) . . ?
C64 C61 P2 107.8(3) . . ?
C62 C61 P2 115.4(4) . . ?
C73 C71 C74 109.3(4) . . ?
C73 C71 C72 108.2(4) . . ?
C74 C71 C72 105.2(4) . . ?
C73 C71 P2 115.1(4) . . ?
C74 C71 P2 107.8(3) . . ?
C72 C71 P2 110.8(4) . . ?
C83 C81 C84 108.1(4) . . ?
C83 C81 C82 108.9(4) . . ?
C84 C81 C82 106.1(4) . . ?
C83 C81 P2 114.6(4) . . ?
C84 C81 P2 110.2(4) . . ?
C82 C81 P2 108.6(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C21 1.965(5) . ?
Pt1 C11 2.295(6) . ?
Pt1 P1 2.3195(13) . ?
Pt1 Ru1 2.6890(4) . ?
Pt1 Ru2 2.8584(5) . ?
Pt2 C25 2.037(5) . ?
Pt2 C23 2.104(5) . ?
Pt2 P2 2.3147(13) . ?
Pt2 Ru2 2.7899(4) . ?
Pt2 Ru1 2.8218(5) . ?
Ru1 C14 1.910(5) . ?
Ru1 C13 1.932(6) . ?
Ru1 C12 1.951(6) . ?
Ru1 C11 1.971(5) . ?
Ru1 Ru2 2.9724(6) . ?
Ru2 C24 1.885(5) . ?
Ru2 C22 1.937(6) . ?
Ru2 C25 2.040(5) . ?
Ru2 C23 2.047(5) . ?
Ru2 C21 2.162(5) . ?
P1 C41 1.905(5) . ?
P1 C51 1.906(5) . ?
P1 C31 1.915(5) . ?
P2 C71 1.906(5) . ?
P2 C61 1.910(5) . ?
P2 C81 1.914(5) . ?
C11 O11 1.154(6) . ?
C12 O12 1.132(6) . ?
C13 O13 1.139(6) . ?
C14 O14 1.135(6) . ?
C21 O21 1.160(6) . ?
C22 O22 1.144(6) . ?
C23 O23 1.164(6) . ?
C24 O24 1.140(6) . ?
C25 O25 1.166(6) . ?
C31 C33 1.521(7) . ?
C31 C32 1.540(8) . ?
C31 C34 1.545(8) . ?
C41 C43 1.521(7) . ?
C41 C44 1.524(7) . ?
C41 C42 1.544(7) . ?
C51 C54 1.527(7) . ?
C51 C52 1.537(7) . ?
C51 C53 1.546(8) . ?
C61 C63 1.527(7) . ?
C61 C64 1.529(7) . ?
C61 C62 1.544(7) . ?
C71 C73 1.527(7) . ?
C71 C74 1.531(7) . ?
C71 C72 1.537(7) . ?
C81 C83 1.526(7) . ?
C81 C84 1.530(7) . ?
C81 C82 1.536(7) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C21 Pt1 Ru1 C14 -143.6(5) . . . . ?
C11 Pt1 Ru1 C14 1.0(5) . . . . ?
P1 Pt1 Ru1 C14 20.5(5) . . . . ?
Ru2 Pt1 Ru1 C14 -179.9(5) . . . . ?
C21 Pt1 Ru1 C13 -54.8(2) . . . . ?
C11 Pt1 Ru1 C13 89.8(2) . . . . ?
P1 Pt1 Ru1 C13 109.29(18) . . . . ?
Ru2 Pt1 Ru1 C13 -91.04(16) . . . . ?
C21 Pt1 Ru1 C12 119.3(2) . . . . ?
C11 Pt1 Ru1 C12 -96.2(2) . . . . ?
P1 Pt1 Ru1 C12 -76.65(17) . . . . ?
Ru2 Pt1 Ru1 C12 83.02(15) . . . . ?
C21 Pt1 Ru1 C11 -144.6(3) . . . . ?
P1 Pt1 Ru1 C11 19.5(2) . . . . ?
Ru2 Pt1 Ru1 C11 179.19(19) . . . . ?
C21 Pt1 Ru1 Pt2 21.02(16) . . . . ?
C11 Pt1 Ru1 Pt2 165.59(19) . . . . ?
P1 Pt1 Ru1 Pt2 -174.90(8) . . . . ?
Ru2 Pt1 Ru1 Pt2 -15.222(14) . . . . ?
C21 Pt1 Ru1 Ru2 36.24(16) . . . . ?
C11 Pt1 Ru1 Ru2 -179.19(19) . . . . ?
P1 Pt1 Ru1 Ru2 -159.67(8) . . . . ?
C25 Pt2 Ru1 C14 -126.1(2) . . . . ?
C23 Pt2 Ru1 C14 148.5(2) . . . . ?
P2 Pt2 Ru1 C14 12.55(16) . . . . ?
Ru2 Pt2 Ru1 C14 -169.07(15) . . . . ?
C25 Pt2 Ru1 C13 140.0(2) . . . . ?
C23 Pt2 Ru1 C13 54.5(2) . . . . ?
P2 Pt2 Ru1 C13 -81.37(17) . . . . ?
Ru2 Pt2 Ru1 C13 97.01(16) . . . . ?
C25 Pt2 Ru1 C12 -35.1(2) . . . . ?
C23 Pt2 Ru1 C12 -120.6(2) . . . . ?
P2 Pt2 Ru1 C12 103.49(16) . . . . ?
Ru2 Pt2 Ru1 C12 -78.13(15) . . . . ?
C25 Pt2 Ru1 C11 114.4(7) . . . . ?
C23 Pt2 Ru1 C11 28.9(7) . . . . ?
P2 Pt2 Ru1 C11 -107.0(6) . . . . ?
Ru2 Pt2 Ru1 C11 71.4(6) . . . . ?
C25 Pt2 Ru1 Pt1 58.70(14) . . . . ?
C23 Pt2 Ru1 Pt1 -26.77(15) . . . . ?
P2 Pt2 Ru1 Pt1 -162.67(6) . . . . ?
Ru2 Pt2 Ru1 Pt1 15.706(15) . . . . ?
C25 Pt2 Ru1 Ru2 42.99(14) . . . . ?
C23 Pt2 Ru1 Ru2 -42.47(15) . . . . ?
P2 Pt2 Ru1 Ru2 -178.38(6) . . . . ?
C25 Pt2 Ru2 C24 75.9(3) . . . . ?
C23 Pt2 Ru2 C24 -60.4(3) . . . . ?
P2 Pt2 Ru2 C24 5.32(19) . . . . ?
Ru1 Pt2 Ru2 C24 -172.96(18) . . . . ?
C25 Pt2 Ru2 C22 -44.0(3) . . . . ?
C23 Pt2 Ru2 C22 179.6(3) . . . . ?
P2 Pt2 Ru2 C22 -114.63(19) . . . . ?
Ru1 Pt2 Ru2 C22 67.10(19) . . . . ?
C23 Pt2 Ru2 C25 -136.3(3) . . . . ?
P2 Pt2 Ru2 C25 -70.6(2) . . . . ?
Ru1 Pt2 Ru2 C25 111.14(19) . . . . ?
C25 Pt2 Ru2 C23 136.3(3) . . . . ?
P2 Pt2 Ru2 C23 65.8(2) . . . . ?
Ru1 Pt2 Ru2 C23 -112.52(19) . . . . ?
C25 Pt2 Ru2 C21 -173.0(3) . . . . ?
C23 Pt2 Ru2 C21 50.6(2) . . . . ?
P2 Pt2 Ru2 C21 116.39(17) . . . . ?
Ru1 Pt2 Ru2 C21 -61.88(16) . . . . ?
C25 Pt2 Ru2 Pt1 -125.40(19) . . . . ?
C23 Pt2 Ru2 Pt1 98.26(19) . . . . ?
P2 Pt2 Ru2 Pt1 164.01(6) . . . . ?
Ru1 Pt2 Ru2 Pt1 -14.259(13) . . . . ?
C25 Pt2 Ru2 Ru1 -111.14(19) . . . . ?
C23 Pt2 Ru2 Ru1 112.52(19) . . . . ?
P2 Pt2 Ru2 Ru1 178.27(6) . . . . ?
C21 Pt1 Ru2 C24 42.4(3) . . . . ?
C11 Pt1 Ru2 C24 172.4(2) . . . . ?
P1 Pt1 Ru2 C24 -21.0(2) . . . . ?
Ru1 Pt1 Ru2 C24 171.79(19) . . . . ?
C21 Pt1 Ru2 C22 122.1(3) . . . . ?
C11 Pt1 Ru2 C22 -107.9(2) . . . . ?
P1 Pt1 Ru2 C22 58.67(16) . . . . ?
Ru1 Pt1 Ru2 C22 -108.51(15) . . . . ?
C21 Pt1 Ru2 C25 -165.5(3) . . . . ?
C11 Pt1 Ru2 C25 -35.5(2) . . . . ?
P1 Pt1 Ru2 C25 131.02(19) . . . . ?
Ru1 Pt1 Ru2 C25 -36.16(18) . . . . ?
C21 Pt1 Ru2 C23 -62.2(3) . . . . ?
C11 Pt1 Ru2 C23 67.8(2) . . . . ?
P1 Pt1 Ru2 C23 -125.62(15) . . . . ?
Ru1 Pt1 Ru2 C23 67.20(15) . . . . ?
C11 Pt1 Ru2 C21 130.0(3) . . . . ?
P1 Pt1 Ru2 C21 -63.4(2) . . . . ?
Ru1 Pt1 Ru2 C21 129.4(2) . . . . ?
C21 Pt1 Ru2 Pt2 -114.5(2) . . . . ?
C11 Pt1 Ru2 Pt2 15.51(15) . . . . ?
P1 Pt1 Ru2 Pt2 -177.93(5) . . . . ?
Ru1 Pt1 Ru2 Pt2 14.883(14) . . . . ?
C21 Pt1 Ru2 Ru1 -129.4(2) . . . . ?
C11 Pt1 Ru2 Ru1 0.62(15) . . . . ?
P1 Pt1 Ru2 Ru1 167.18(5) . . . . ?
C14 Ru1 Ru2 C24 83.1(14) . . . . ?
C13 Ru1 Ru2 C24 -9.6(14) . . . . ?
C12 Ru1 Ru2 C24 169.6(14) . . . . ?
C11 Ru1 Ru2 C24 -97.5(14) . . . . ?
Pt1 Ru1 Ru2 C24 -96.8(14) . . . . ?
Pt2 Ru1 Ru2 C24 67.0(14) . . . . ?
C14 Ru1 Ru2 C22 -116.6(3) . . . . ?
C13 Ru1 Ru2 C22 150.7(2) . . . . ?
C12 Ru1 Ru2 C22 -30.2(2) . . . . ?
C11 Ru1 Ru2 C22 62.7(2) . . . . ?
Pt1 Ru1 Ru2 C22 63.47(14) . . . . ?
Pt2 Ru1 Ru2 C22 -132.78(14) . . . . ?
C14 Ru1 Ru2 C25 -27.1(3) . . . . ?
C13 Ru1 Ru2 C25 -119.8(2) . . . . ?
C12 Ru1 Ru2 C25 59.3(2) . . . . ?
C11 Ru1 Ru2 C25 152.2(2) . . . . ?
Pt1 Ru1 Ru2 C25 152.95(14) . . . . ?
Pt2 Ru1 Ru2 C25 -43.30(14) . . . . ?
C14 Ru1 Ru2 C23 60.4(3) . . . . ?
C13 Ru1 Ru2 C23 -32.3(2) . . . . ?
C12 Ru1 Ru2 C23 146.8(2) . . . . ?
C11 Ru1 Ru2 C23 -120.3(2) . . . . ?
Pt1 Ru1 Ru2 C23 -119.57(14) . . . . ?
Pt2 Ru1 Ru2 C23 44.19(14) . . . . ?
C14 Ru1 Ru2 C21 147.8(3) . . . . ?
C13 Ru1 Ru2 C21 55.1(2) . . . . ?
C12 Ru1 Ru2 C21 -125.8(2) . . . . ?
C11 Ru1 Ru2 C21 -32.9(2) . . . . ?
Pt1 Ru1 Ru2 C21 -32.13(14) . . . . ?
Pt2 Ru1 Ru2 C21 131.62(14) . . . . ?
C14 Ru1 Ru2 Pt2 16.2(2) . . . . ?
C13 Ru1 Ru2 Pt2 -76.53(15) . . . . ?
C12 Ru1 Ru2 Pt2 102.59(16) . . . . ?
C11 Ru1 Ru2 Pt2 -164.51(18) . . . . ?
Pt1 Ru1 Ru2 Pt2 -163.753(15) . . . . ?
C14 Ru1 Ru2 Pt1 179.9(2) . . . . ?
C13 Ru1 Ru2 Pt1 87.22(15) . . . . ?
C12 Ru1 Ru2 Pt1 -93.66(16) . . . . ?
C11 Ru1 Ru2 Pt1 -0.76(18) . . . . ?
Pt2 Ru1 Ru2 Pt1 163.753(15) . . . . ?
C21 Pt1 P1 C41 91.4(2) . . . . ?
C11 Pt1 P1 C41 -57.5(2) . . . . ?
Ru1 Pt1 P1 C41 -72.3(2) . . . . ?
Ru2 Pt1 P1 C41 135.90(17) . . . . ?
C21 Pt1 P1 C51 -30.0(3) . . . . ?
C11 Pt1 P1 C51 -178.9(2) . . . . ?
Ru1 Pt1 P1 C51 166.33(18) . . . . ?
Ru2 Pt1 P1 C51 14.5(2) . . . . ?
C21 Pt1 P1 C31 -149.7(3) . . . . ?
C11 Pt1 P1 C31 61.4(2) . . . . ?
Ru1 Pt1 P1 C31 46.6(2) . . . . ?
Ru2 Pt1 P1 C31 -105.21(19) . . . . ?
C25 Pt2 P2 C71 58.6(2) . . . . ?
C23 Pt2 P2 C71 157.1(2) . . . . ?
Ru2 Pt2 P2 C71 109.50(18) . . . . ?
Ru1 Pt2 P2 C71 -73.34(19) . . . . ?
C25 Pt2 P2 C61 176.3(2) . . . . ?
C23 Pt2 P2 C61 -85.2(2) . . . . ?
Ru2 Pt2 P2 C61 -132.82(17) . . . . ?
Ru1 Pt2 P2 C61 44.33(19) . . . . ?
C25 Pt2 P2 C81 -63.0(2) . . . . ?
C23 Pt2 P2 C81 35.5(2) . . . . ?
Ru2 Pt2 P2 C81 -12.1(2) . . . . ?
Ru1 Pt2 P2 C81 165.11(18) . . . . ?
C14 Ru1 C11 O11 -10.3(10) . . . . ?
C13 Ru1 C11 O11 81.5(10) . . . . ?
C12 Ru1 C11 O11 -103.8(10) . . . . ?
Pt1 Ru1 C11 O11 169.4(10) . . . . ?
Pt2 Ru1 C11 O11 106.5(10) . . . . ?
Ru2 Ru1 C11 O11 170.2(9) . . . . ?
C14 Ru1 C11 Pt1 -179.69(16) . . . . ?
C13 Ru1 C11 Pt1 -87.95(19) . . . . ?
C12 Ru1 C11 Pt1 86.78(18) . . . . ?
Pt2 Ru1 C11 Pt1 -62.9(7) . . . . ?
Ru2 Ru1 C11 Pt1 0.79(19) . . . . ?
C21 Pt1 C11 O11 -121.2(6) . . . . ?
P1 Pt1 C11 O11 15.8(6) . . . . ?
Ru1 Pt1 C11 O11 -172.9(7) . . . . ?
Ru2 Pt1 C11 O11 -173.7(5) . . . . ?
C21 Pt1 C11 Ru1 51.7(3) . . . . ?
P1 Pt1 C11 Ru1 -171.31(9) . . . . ?
Ru2 Pt1 C11 Ru1 -0.79(19) . . . . ?
C14 Ru1 C12 O12 -107(25) . . . . ?
C13 Ru1 C12 O12 124(24) . . . . ?
C11 Ru1 C12 O12 -1(25) . . . . ?
Pt1 Ru1 C12 O12 55(25) . . . . ?
Pt2 Ru1 C12 O12 172(100) . . . . ?
Ru2 Ru1 C12 O12 116(25) . . . . ?
C14 Ru1 C13 O13 74(14) . . . . ?
C12 Ru1 C13 O13 -156(13) . . . . ?
C11 Ru1 C13 O13 -31(14) . . . . ?
Pt1 Ru1 C13 O13 -88(14) . . . . ?
Pt2 Ru1 C13 O13 155(14) . . . . ?
Ru2 Ru1 C13 O13 -148(14) . . . . ?
C13 Ru1 C14 O14 -78(7) . . . . ?
C12 Ru1 C14 O14 107(7) . . . . ?
C11 Ru1 C14 O14 11(7) . . . . ?
Pt1 Ru1 C14 O14 10(7) . . . . ?
Pt2 Ru1 C14 O14 -156(7) . . . . ?
Ru2 Ru1 C14 O14 -170(7) . . . . ?
C11 Pt1 C21 O21 87.7(7) . . . . ?
P1 Pt1 C21 O21 -50.7(7) . . . . ?
Ru1 Pt1 C21 O21 122.3(6) . . . . ?
Ru2 Pt1 C21 O21 167.4(8) . . . . ?
C11 Pt1 C21 Ru2 -79.7(3) . . . . ?
P1 Pt1 C21 Ru2 141.91(11) . . . . ?
Ru1 Pt1 C21 Ru2 -45.02(16) . . . . ?
C24 Ru2 C21 O21 46.1(7) . . . . ?
C22 Ru2 C21 O21 139.6(7) . . . . ?
C25 Ru2 C21 O21 -103.4(10) . . . . ?
C23 Ru2 C21 O21 -43.3(7) . . . . ?
Pt2 Ru2 C21 O21 -78.9(7) . . . . ?
Pt1 Ru2 C21 O21 -167.1(8) . . . . ?
Ru1 Ru2 C21 O21 -127.8(7) . . . . ?
C24 Ru2 C21 Pt1 -146.8(2) . . . . ?
C22 Ru2 C21 Pt1 -53.3(2) . . . . ?
C25 Ru2 C21 Pt1 63.7(10) . . . . ?
C23 Ru2 C21 Pt1 123.8(2) . . . . ?
Pt2 Ru2 C21 Pt1 88.23(17) . . . . ?
Ru1 Ru2 C21 Pt1 39.31(15) . . . . ?
C24 Ru2 C22 O22 -57(5) . . . . ?
C25 Ru2 C22 O22 43(5) . . . . ?
C23 Ru2 C22 O22 77(6) . . . . ?
C21 Ru2 C22 O22 -148(5) . . . . ?
Pt2 Ru2 C22 O22 73(5) . . . . ?
Pt1 Ru2 C22 O22 176(5) . . . . ?
Ru1 Ru2 C22 O22 125(5) . . . . ?
C24 Ru2 C23 O23 -54.2(9) . . . . ?
C22 Ru2 C23 O23 171(2) . . . . ?
C25 Ru2 C23 O23 -154.2(9) . . . . ?
C21 Ru2 C23 O23 36.5(9) . . . . ?
Pt2 Ru2 C23 O23 175.5(10) . . . . ?
Pt1 Ru2 C23 O23 73.9(9) . . . . ?
Ru1 Ru2 C23 O23 123.2(9) . . . . ?
C24 Ru2 C23 Pt2 130.2(2) . . . . ?
C22 Ru2 C23 Pt2 -4(3) . . . . ?
C25 Ru2 C23 Pt2 30.26(18) . . . . ?
C21 Ru2 C23 Pt2 -139.08(19) . . . . ?
Pt1 Ru2 C23 Pt2 -101.63(13) . . . . ?
Ru1 Ru2 C23 Pt2 -52.36(12) . . . . ?
C25 Pt2 C23 O23 152.3(5) . . . . ?
P2 Pt2 C23 O23 33.9(5) . . . . ?
Ru2 Pt2 C23 O23 -177.4(6) . . . . ?
Ru1 Pt2 C23 O23 -121.2(5) . . . . ?
C25 Pt2 C23 Ru2 -30.36(18) . . . . ?
P2 Pt2 C23 Ru2 -148.73(9) . . . . ?
Ru1 Pt2 C23 Ru2 56.20(13) . . . . ?
C22 Ru2 C24 O24 -147(16) . . . . ?
C25 Ru2 C24 O24 123(16) . . . . ?
C23 Ru2 C24 O24 36(16) . . . . ?
C21 Ru2 C24 O24 -51(16) . . . . ?
Pt2 Ru2 C24 O24 77(16) . . . . ?
Pt1 Ru2 C24 O24 -78(16) . . . . ?
Ru1 Ru2 C24 O24 14(17) . . . . ?
C23 Pt2 C25 O25 -154.5(5) . . . . ?
P2 Pt2 C25 O25 -37.9(5) . . . . ?
Ru2 Pt2 C25 O25 175.2(6) . . . . ?
Ru1 Pt2 C25 O25 118.0(5) . . . . ?
C23 Pt2 C25 Ru2 30.38(19) . . . . ?
P2 Pt2 C25 Ru2 146.91(9) . . . . ?
Ru1 Pt2 C25 Ru2 -57.11(13) . . . . ?
C24 Ru2 C25 O25 66.9(8) . . . . ?
C22 Ru2 C25 O25 -26.5(8) . . . . ?
C23 Ru2 C25 O25 155.8(8) . . . . ?
C21 Ru2 C25 O25 -144.1(8) . . . . ?
Pt2 Ru2 C25 O25 -172.9(9) . . . . ?
Pt1 Ru2 C25 O25 -90.4(8) . . . . ?
Ru1 Ru2 C25 O25 -119.5(8) . . . . ?
C24 Ru2 C25 Pt2 -120.2(2) . . . . ?
C22 Ru2 C25 Pt2 146.4(2) . . . . ?
C23 Ru2 C25 Pt2 -31.28(19) . . . . ?
C21 Ru2 C25 Pt2 28.9(10) . . . . ?
Pt1 Ru2 C25 Pt2 82.54(19) . . . . ?
Ru1 Ru2 C25 Pt2 53.39(12) . . . . ?
C41 P1 C31 C33 -41.9(5) . . . . ?
C51 P1 C31 C33 73.9(5) . . . . ?
Pt1 P1 C31 C33 -162.3(4) . . . . ?
C41 P1 C31 C32 80.9(4) . . . . ?
C51 P1 C31 C32 -163.3(4) . . . . ?
Pt1 P1 C31 C32 -39.5(4) . . . . ?
C41 P1 C31 C34 -164.2(4) . . . . ?
C51 P1 C31 C34 -48.4(4) . . . . ?
Pt1 P1 C31 C34 75.4(4) . . . . ?
C51 P1 C41 C43 -163.3(4) . . . . ?
C31 P1 C41 C43 -47.3(4) . . . . ?
Pt1 P1 C41 C43 71.4(4) . . . . ?
C51 P1 C41 C44 -40.6(5) . . . . ?
C31 P1 C41 C44 75.4(4) . . . . ?
Pt1 P1 C41 C44 -165.9(3) . . . . ?
C51 P1 C41 C42 82.6(4) . . . . ?
C31 P1 C41 C42 -161.4(4) . . . . ?
Pt1 P1 C41 C42 -42.7(4) . . . . ?
C41 P1 C51 C54 76.1(5) . . . . ?
C31 P1 C51 C54 -40.5(5) . . . . ?
Pt1 P1 C51 C54 -160.6(4) . . . . ?
C41 P1 C51 C52 -162.0(4) . . . . ?
C31 P1 C51 C52 81.4(4) . . . . ?
Pt1 P1 C51 C52 -38.7(4) . . . . ?
C41 P1 C51 C53 -46.5(4) . . . . ?
C31 P1 C51 C53 -163.1(4) . . . . ?
Pt1 P1 C51 C53 76.8(4) . . . . ?
C71 P2 C61 C63 45.4(4) . . . . ?
C81 P2 C61 C63 164.8(4) . . . . ?
Pt2 P2 C61 C63 -71.9(4) . . . . ?
C71 P2 C61 C64 160.3(4) . . . . ?
C81 P2 C61 C64 -80.3(4) . . . . ?
Pt2 P2 C61 C64 43.0(4) . . . . ?
C71 P2 C61 C62 -77.2(4) . . . . ?
C81 P2 C61 C62 42.2(4) . . . . ?
Pt2 P2 C61 C62 165.5(3) . . . . ?
C61 P2 C71 C73 40.8(5) . . . . ?
C81 P2 C71 C73 -78.4(4) . . . . ?
Pt2 P2 C71 C73 157.8(4) . . . . ?
C61 P2 C71 C74 -81.5(4) . . . . ?
C81 P2 C71 C74 159.3(4) . . . . ?
Pt2 P2 C71 C74 35.5(4) . . . . ?
C61 P2 C71 C72 164.0(4) . . . . ?
C81 P2 C71 C72 44.8(4) . . . . ?
Pt2 P2 C71 C72 -79.1(4) . . . . ?
C71 P2 C81 C83 43.3(5) . . . . ?
C61 P2 C81 C83 -75.8(4) . . . . ?
Pt2 P2 C81 C83 164.2(3) . . . . ?
C71 P2 C81 C84 165.4(4) . . . . ?
C61 P2 C81 C84 46.3(4) . . . . ?
Pt2 P2 C81 C84 -73.7(4) . . . . ?
C71 P2 C81 C82 -78.8(4) . . . . ?
C61 P2 C81 C82 162.1(3) . . . . ?
Pt2 P2 C81 C82 42.1(4) . . . . ?
