Crystallography Open Database

Information card for entry 4312283

Preview

Coordinates	4312283.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C150 H140 N6 O19 P6 Rh6
Calculated formula	C150 H114 N6 O18.99 P6 Rh6
Title of publication	Chiral Organometallic Triangles with Rh-Rh Bonds. 1. Compounds Prepared from Racemic cis-Rh2(C6H4PPh2)2(OAc)2
Authors of publication	F. Albert Cotton; Carlos A. Murillo; Xiaoping Wang; Rongmin Yu
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	8394 - 8403
a	19.1896 ± 0.0004 Å
b	19.1896 ± 0.0004 Å
c	21.0249 ± 0.0009 Å
α	90°
β	90°
γ	120°
Cell volume	6705 ± 0.3 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	6
Space group number	163
Hermann-Mauguin space group symbol	P -3 1 c
Hall space group symbol	-P 3 2c
Residual factor for all reflections	0.0432
Residual factor for significantly intense reflections	0.0308
Weighted residual factors for significantly intense reflections	0.08
Weighted residual factors for all reflections included in the refinement	0.0931
Goodness-of-fit parameter for all reflections included in the refinement	1.145
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179161 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/22.	4312283.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4312283.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4312283.cif
3788	2010-11-17	../uploads/cif-deposit/cod/cif Adding structures of 4312283 via cif-deposit CGI script.	4312283.cif