Crystallography Open Database

Information card for entry 4313252

Preview

Coordinates	4313252.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 Cl10 Re2 S2
Calculated formula	C24 H35 Cl10 Re2 S2
Title of publication	Syntheses of a Cp'ReS Derivative and More Complex Products
Authors of publication	S. H. Pawlicki; B. C. Noll; J. A. Kanney; M. Rakowski DuBois
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	1556 - 1563
a	17.974 ± 0.0006 Å
b	8.1844 ± 0.0003 Å
c	23.6931 ± 0.0008 Å
α	90°
β	93.098 ± 0.001°
γ	90°
Cell volume	3480.3 ± 0.2 Å³
Cell temperature	409 ± 2 K
Ambient diffraction temperature	137 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0485
Residual factor for significantly intense reflections	0.0429
Weighted residual factors for significantly intense reflections	0.11
Weighted residual factors for all reflections included in the refinement	0.1135
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179188 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/32.	4313252.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313252.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313252.cif
6321	2011-01-11	../uploads/cif-deposit/cod/cif Adding structures of 4313252 via cif-deposit CGI script.	4313252.cif