Crystallography Open Database

Information card for entry 4313358

Preview

Coordinates	4313358.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H20 Cl4 Ga2 N2
Calculated formula	C8 H20 Cl4 Ga2 N2
SMILES	[NH]1(C(C)(C)C)[Ga](Cl)([NH](C(C)(C)C)[Ga]1(Cl)Cl)Cl
Title of publication	Syntheses and X-ray Structures of Monocyclic, Bicyclic, and Spirocyclic Gallium and Indium Boraamidinates
Authors of publication	Tristram Chivers; Chantall Fedorchuk; Gabriele Schatte; Masood Parvez
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	2084 - 2093
a	6.467 ± 0.0002 Å
b	11.86 ± 0.0005 Å
c	10.742 ± 0.0005 Å
α	90°
β	96.379 ± 0.0014°
γ	90°
Cell volume	818.8 ± 0.06 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0699
Residual factor for significantly intense reflections	0.0392
Weighted residual factors for significantly intense reflections	0.0859
Weighted residual factors for all reflections included in the refinement	0.0976
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179191 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/33.	4313358.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313358.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313358.cif
6427	2011-01-11	../uploads/cif-deposit/cod/cif Adding structures of 4313358 via cif-deposit CGI script.	4313358.cif