Crystallography Open Database

Information card for entry 4314611

Preview

Coordinates	4314611.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H23 Br N2 Si
Calculated formula	C15 H23 Br N2 Si
Title of publication	Reactivity of a Disilylene [{PhC(NBut)2}Si]2 toward Bromine: Synthesis and Characterization of a Stable Monomeric Bromosilylene
Authors of publication	Hui-Xian Yeong; Kai-Chung Lau; Hong-Wei Xi; Kok Hwa Lim; Cheuk-Wai So
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	371 - 373
a	14.2389 ± 0.0011 Å
b	11.1641 ± 0.0008 Å
c	11.9823 ± 0.0009 Å
α	90°
β	116.28 ± 0.004°
γ	90°
Cell volume	1707.9 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0957
Residual factor for significantly intense reflections	0.0636
Weighted residual factors for significantly intense reflections	0.1665
Weighted residual factors for all reflections included in the refinement	0.1899
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179224 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/46.	4314611.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4314611.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4314611.cif
7754	2011-02-02	../uploads/cif-deposit/cod/cif Adding structures of 4314611 via cif-deposit CGI script.	4314611.cif