Crystallography Open Database

Information card for entry 4315764

Preview

Coordinates	4315764.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H47 N3 Pb
Calculated formula	C31 H47 N3 Pb
Title of publication	Synthesis and Reaction of Monomeric Germanium(II) and Lead(II) Dimethylamide and the Synthesis of Germanium(II) Hydrazide by Clevage of one N-H bond of Hydrazine
Authors of publication	Anukul Jana; Herbert W. Roesky; Carola Schulzke; Prinson P. Samuel; Alexander Döring
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	5554 - 5559
a	8.9507 ± 0.0018 Å
b	22.604 ± 0.005 Å
c	14.904 ± 0.003 Å
α	90°
β	99.12 ± 0.03°
γ	90°
Cell volume	2977.3 ± 1.1 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	4
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0679
Residual factor for significantly intense reflections	0.0667
Weighted residual factors for significantly intense reflections	0.1752
Weighted residual factors for all reflections included in the refinement	0.1766
Goodness-of-fit parameter for all reflections included in the refinement	1.143
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179237 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/57.	4315764.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4315764.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4315764.cif
8924	2011-02-08	../uploads/cif-deposit/cod/cif Adding structures of 4315764 via cif-deposit CGI script.	4315764.cif