Crystallography Open Database

Information card for entry 4317504

Preview

Coordinates	4317504.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C92 H90 N12 O8 P4 Rh2
Calculated formula	C92 H85 N12 O8 P4 Rh2
Title of publication	Oxidative Addition of N-H Bonds to a Metal Center: Synthesis, Characterization, and Crystal Structure of New Rhodium(III) Hydrido-Pyrazolate Complexes
Authors of publication	G. Attilio Ardizzoia; Stefano Brenna; Girolamo LaMonica; Angelo Maspero; Norberto Masciocchi; Massimo Moret
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	610 - 614
a	12.537 ± 0.002 Å
b	18.113 ± 0.003 Å
c	38.231 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	8682 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P b n 21
Hall space group symbol	P 2c -2ab
Residual factor for all reflections	0.0472
Residual factor for significantly intense reflections	0.0472
Weighted residual factors for significantly intense reflections	0.0896
Weighted residual factors for all reflections included in the refinement	0.0896
Goodness-of-fit parameter for all reflections included in the refinement	1.124
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179255 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/75.	4317504.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317504.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317504.cif
12240	2011-03-05	../uploads/cif-deposit/cod/cif Adding structures of 4317504 via cif-deposit CGI script.	4317504.cif