Crystallography Open Database

Information card for entry 4317516

Preview

Coordinates	4317516.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H60 N10 Te11.57 Tm4
Calculated formula	C62 H60 N10 Te11.57 Tm4
Title of publication	Chalcogen-Rich Lanthanide Clusters: Compounds with Te2-, (TeTe)2-, TePh, TeTePh, (TeTeTe(Ph)TeTe)5-, and [(TeTe)4TePh]9- Ligands; Single Source Precursors to Solid-State Lanthanide Tellurides
Authors of publication	Deborah Freedman; Thomas J. Emge; John G. Brennan
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	492 - 500
a	23.407 ± 0.007 Å
b	23.2 ± 0.02 Å
c	17.507 ± 0.009 Å
α	90 ± 0.06°
β	113.38 ± 0.04°
γ	90 ± 0.04°
Cell volume	8726 ± 10 Å³
Cell temperature	153 ± 5 K
Ambient diffraction temperature	153 ± 5 K
Number of distinct elements	5
Space group number	5
Hermann-Mauguin space group symbol	C 1 2 1
Hall space group symbol	C 2y
Residual factor for all reflections	0.1569
Residual factor for significantly intense reflections	0.0877
Weighted residual factors for significantly intense reflections	0.2149
Weighted residual factors for all reflections included in the refinement	0.2403
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179255 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/75.	4317516.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317516.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317516.cif
12264	2011-03-05	../uploads/cif-deposit/cod/cif Adding structures of 4317516 via cif-deposit CGI script.	4317516.cif