Crystallography Open Database

Information card for entry 4317523

Preview

Coordinates	4317523.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C142 H209.5 Al3 N6 O19 P3
Calculated formula	C142 H209.52 Al3 N6 O19 P3
Title of publication	Ligand-Tetrahydrofuran Coupling in Chelated Aluminum Phosphinates
Authors of publication	Y. Wang; S. Parkin; D. Atwood
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	558 - 565
a	16.65 ± 0.001 Å
b	27.518 ± 0.002 Å
c	31.149 ± 0.002 Å
α	90°
β	92.28 ± 0.01°
γ	90°
Cell volume	14260.4 ± 1.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1059
Residual factor for significantly intense reflections	0.0765
Weighted residual factors for significantly intense reflections	0.1896
Weighted residual factors for all reflections included in the refinement	0.2078
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4317523.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317523.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317523.cif
12278	2011-03-05	../uploads/cif-deposit/cod/cif Adding structures of 4317523 via cif-deposit CGI script.	4317523.cif