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Information card for entry 4317534
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| Coordinates | 4317534.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | SnPh2Cl2.VO(acetophen1,2pn) |
|---|---|
| Chemical name | Diphenyltin dichloride.[N,N'-bis(alpha-methylsalicylidene)ethane-1,2-diaminato]oxo vanadium(IV) (1/1) |
| Formula | C32 H32 Cl4 N2 O3 Sn V |
| Calculated formula | C32 H32 Cl4 N2 O3 Sn V |
| Title of publication | Donor Properties of the Vanadyl Ion: Reactions of Vanadyl Salicylaldimine β-Ketimine and Acetylacetonato Complexes with Groups 14 and 15 Lewis Acids |
| Authors of publication | B. Cashin; D. Cunningham; P. Daly; P. McArdle; M. Munroe; N. Ní Chonchubhair |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2002 |
| Journal volume | 41 |
| Pages of publication | 773 - 782 |
| a | 11.184 ± 0.004 Å |
| b | 17.181 ± 0.003 Å |
| c | 17.528 ± 0.002 Å |
| α | 89.988 ± 0.013° |
| β | 92.178 ± 0.018° |
| γ | 90.006 ± 0.019° |
| Cell volume | 3365.6 ± 1.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.143 |
| Residual factor for significantly intense reflections | 0.0966 |
| Weighted residual factors for significantly intense reflections | 0.2356 |
| Weighted residual factors for all reflections included in the refinement | 0.2628 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.968 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288183 (current) | 2023-12-08 | cod/ Corrected misspelt data names in multiple entries using the 'cif_correct_tags' program and a data names replacement file from cod-tools revision 9827. This change affected only the misspelt variants of the '_atom_site_symmetry_multiplicity' data name. |
4317534.cif |
| 179255 | 2016-03-23 | cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/75. |
4317534.cif |
| 120093 | 2014-07-12 | Adding DOIs to range 4/31 structures. | 4317534.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4317534.cif |
| 17004 | 2011-03-31 | cif/ Commiting CIFs, that were updated with the 'cif_fix_values' script, using options '--fix-misspelled replacement_values.lst', '--fix-temperature' and '--fix-enums' with built-in table of enum values. The following cmd was used: > (set -x; find ? -name \*.cif | sort | xargs -i sh -c 'if !( > cif_fix_values --fix-misspelled ~/../inputs/replacament_values.lst {} | > cif_filter --add-cif-header {} | > sponge {} ) 2>&1 | grep NOTE; then svn revert {}; > fi' ) & |
4317534.cif |
| 13809 | 2011-03-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4317534 via cif-deposit CGI script. |
4317534.cif |
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