Crystallography Open Database

Information card for entry 4318144

Preview

Coordinates	4318144.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H88 Cl3 La N16 O24
Calculated formula	C64 H68 Cl3 La N16 O24
Title of publication	Synthesis, Structures, and Magnetic Properties of a Series of Lanthanum(III) and Gadolinium(III) Complexes with Chelating Benzimidazole-Substituted Nitronyl Nitroxide Free Radicals. Evidence for Antiferromagnetic GdIII-Radical Interactions
Authors of publication	Christophe Lescop; Elie Belorizky; Dominique Luneau; Paul Rey
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	3375 - 3384
a	11.0682 ± 0.0008 Å
b	34.24 ± 0.003 Å
c	42.787 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	16215 ± 2 Å³
Cell temperature	143 ± 2 K
Ambient diffraction temperature	143 ± 2 K
Number of distinct elements	6
Space group number	70
Hermann-Mauguin space group symbol	F d d d :1
Hall space group symbol	F 2 2 -1d
Residual factor for all reflections	0.0965
Residual factor for significantly intense reflections	0.0876
Weighted residual factors for significantly intense reflections	0.2281
Weighted residual factors for all reflections included in the refinement	0.2336
Goodness-of-fit parameter for all reflections included in the refinement	1.995
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179261 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/81.	4318144.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4318144.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4318144.cif
14432	2011-03-10	../uploads/cif-deposit/cod/cif Adding structures of 4318144 via cif-deposit CGI script.	4318144.cif