Crystallography Open Database

Information card for entry 4318697

Preview

Coordinates	4318697.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69.25 H60.5 Cl0.5 O8 Ru5 Sn4
Calculated formula	C69.25 H60.5 Cl0.5 O8 Ru5 Sn4
Title of publication	High Nuclearity Ruthenium-Tin Clusters from the Reactions of Triphenylstannane with Pentaruthenium Carbonyl Carbido Cluster Complexes
Authors of publication	Richard D. Adams; Burjor Captain; Wei Fu; Mark D. Smith
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	5593 - 5601
a	14.6107 ± 0.0011 Å
b	18.7109 ± 0.0014 Å
c	25.3931 ± 0.0019 Å
α	90°
β	102.812 ± 0.001°
γ	90°
Cell volume	6769.1 ± 0.9 Å³
Cell temperature	190 ± 2 K
Ambient diffraction temperature	190 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0727
Residual factor for significantly intense reflections	0.0595
Weighted residual factors for significantly intense reflections	0.1488
Weighted residual factors for all reflections included in the refinement	0.155
Goodness-of-fit parameter for all reflections included in the refinement	1.143
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4318697.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4318697.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4318697.cif
15418	2011-03-16	../uploads/cif-deposit/cod/cif Adding structures of 4318697 via cif-deposit CGI script.	4318697.cif