Crystallography Open Database

Information card for entry 4319112

4319111 << 4319112 >> 4319113

Preview

Coordinates	4319112.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H60 Ho2 N10 Te2
Calculated formula	C66 H60 Ho2 N10 Te2
Title of publication	Heteroleptic Lanthanide Compounds with Chalcogenolate Ligands: Reduction of PhNNPh/PhEEPh (E = Se or Te) Mixtures with Ln (Ln = Ho, Er, Tm, Yb). Thermolysis Can Give LnN or LnE
Authors of publication	Anna Kornienko; Deborah Freedman; Thomas J. Emge; John G. Brennan
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	140 - 145
a	10.349 ± 0.002 Å
b	17.662 ± 0.004 Å
c	17.73 ± 0.008 Å
α	75.82 ± 0.03°
β	74.11 ± 0.03°
γ	89.45 ± 0.02°
Cell volume	3016.2 ± 1.8 Å³
Cell temperature	153 ± 5 K
Ambient diffraction temperature	153 ± 5 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0651
Residual factor for significantly intense reflections	0.0323
Weighted residual factors for significantly intense reflections	0.0693
Weighted residual factors for all reflections included in the refinement	0.074
Goodness-of-fit parameter for all reflections included in the refinement	0.998
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179271 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/91.	4319112.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4319112.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4319112.cif
15844	2011-03-18	../uploads/cif-deposit/cod/cif Adding structures of 4319112 via cif-deposit CGI script.	4319112.cif