Crystallography Open Database

Information card for entry 4319972

4319971 << 4319972 >> 4319973

Preview

Coordinates	4319972.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H26 Br2 Cl5 Cu N4 O2.5 Zn
Calculated formula	C23 H25 Br2 Cl5 Cu N4 O2.5 Zn
Title of publication	Tetranuclear Mixed-Metal MII2CuII2 Complexes Derived from a Phenol-Based Macrocyclic Ligand Having Two N(amine)2O2 and Two N(imine)2O2 Metal-Binding Sites
Authors of publication	Yuki Nakamura; Masami Yonemura; Keisuke Arimura; Naoki Usuki; Masaaki Ohba; Hisashi Ōkawa
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	3739 - 3744
a	32.53 ± 0.01 Å
b	12.242 ± 0.002 Å
c	19.729 ± 0.009 Å
α	90°
β	126.03 ± 0.03°
γ	90°
Cell volume	6354 ± 4 Å³
Cell temperature	296.2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0559
Weighted residual factors for all reflections included in the refinement	0.0734
Goodness-of-fit parameter for all reflections included in the refinement	1.764
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4319972.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4319972.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4319972.cif
16777	2011-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4319972 via cif-deposit CGI script.	4319972.cif