Crystallography Open Database

Information card for entry 4319975

4319974 << 4319975 >> 4319976

Preview

Coordinates	4319975.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H64 Cl2 N6 Ni P2 S2
Calculated formula	C41 H64 Cl2 N6 Ni P2 S2
Title of publication	Contrasting Formation of a (Phenylthio)phosphinimine and (Phenylthio)phosphazide. Synthesis of Metal Complexes
Authors of publication	Luc LePichon; Douglas W. Stephan
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	3827 - 3829
a	21.5918 ± 0.0002 Å
b	10.6069 ± 0.0001 Å
c	22.7952 ± 0.0001 Å
α	90°
β	106.312 ± 0.001°
γ	90°
Cell volume	5010.46 ± 0.07 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1586
Residual factor for significantly intense reflections	0.0869
Weighted residual factors for significantly intense reflections	0.1957
Weighted residual factors for all reflections included in the refinement	0.2303
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179279 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/99.	4319975.cif
132087	2015-02-19	cif/ (antanas@koala.ibt.lt) Replacing '_chemical_name_systematic' tag values consisting ';' with '?'.	4319975.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4319975.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4319975.cif
16780	2011-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4319975 via cif-deposit CGI script.	4319975.cif