Crystallography Open Database

Information card for entry 4320268

4320267 << 4320268 >> 4320269

Preview

Coordinates	4320268.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H56 N2 O Si2 Zn
Calculated formula	C33 H56 N2 O Si2 Zn
SMILES	[Zn]1(Oc2c(cc(cc2C=[N]1c1c(cccc1C(C)C)C(C)C)C(C)(C)C)C(C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
Title of publication	Three-Coordinate Zinc Amide and Phenoxide Complexes Supported by a Bulky Schiff Base Ligand
Authors of publication	Malcolm H. Chisholm; Judith C. Gallucci; Hongshi Zhen; John C. Huffman
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5051 - 5054
a	10.7872 ± 0.0003 Å
b	10.8787 ± 0.0003 Å
c	17.447 ± 0.0005 Å
α	78.847 ± 0.0012°
β	88.3583 ± 0.0011°
γ	64.1491 ± 0.0013°
Cell volume	1804.14 ± 0.09 Å³
Cell temperature	113 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.028
Weighted residual factors for all reflections included in the refinement	0.0321
Goodness-of-fit parameter for all reflections included in the refinement	0.7396
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4320268.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320268.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320268.cif
17170	2011-04-04	../uploads/cif-deposit/cod/cif Adding structures of 4320268 via cif-deposit CGI script.	4320268.cif