#------------------------------------------------------------------------------ #$Date: 2012-02-04 18:30:22 +0200 (Sat, 04 Feb 2012) $ #$Revision: 32116 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/4320274.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4320274 loop_ _publ_author_name 'Bouchra El Mouatassim' 'C\'eline Pearson' 'Alan Shaver' _publ_section_title ; The Preparation of (\h5-C5Me5)Ir(PMe3)S4 from (\h5-C5Me5)Ir(PMe3)(SH)2 and SO2 ; _journal_name_full 'Inorganic Chemistry' _journal_page_first 5290 _journal_page_last 5291 _journal_volume 40 _journal_year 2001 _chemical_compound_source 'synthesized by the authors, see text' _chemical_formula_moiety 'C13 H24 Ir P S4' _chemical_formula_structural Ir(PCH3)(Cp*)(S4) _chemical_formula_sum 'C13 H24 Ir P S4' _chemical_formula_weight 531.75 _chemical_name_systematic ; ? ; _space_group_IT_number 19 _symmetry_cell_setting orthorhombic _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method 'SHELXL96 (Sheldrick, 1996)' _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 8.767(3) _cell_length_b 13.443(5) _cell_length_c 15.447(4) _cell_measurement_reflns_used 25 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 17.5 _cell_measurement_theta_min 12.5 _cell_volume 1820.5(10) _shelx_title ' COLLECTION COMPLETE' _shelx_refln_list_code 4 _shelx_F_calc_maximum 343.57 _exptl_crystal_F_000 1032.00 _reflns_d_resolution_high 0.8099 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16159.86 18619.38 125.05 o 4 0 0 45255.70 45197.69 279.49 o 6 0 0 23079.32 22004.85 272.09 o 8 0 0 285.71 194.44 167.22 o 10 0 0 5090.62 4745.12 282.43 o 1 1 0 36089.36 38176.88 113.71 o 2 1 0 27175.35 27311.84 123.97 o 3 1 0 34683.05 36985.95 174.38 o 4 1 0 3177.55 2835.14 74.86 o 5 1 0 1.99 15.55 73.02 o 6 1 0 827.26 833.22 92.92 o 7 1 0 6827.11 5701.23 157.57 o 8 1 0 1648.47 1607.47 129.67 o 9 1 0 3938.60 3788.62 170.38 o 10 1 0 4.09 341.75 154.24 o 0 2 0 96078.96 88567.93 222.88 o 1 2 0 30647.87 34132.64 127.96 o 2 2 0 13960.08 14495.68 103.99 o 3 2 0 3663.14 4637.79 74.91 o 4 2 0 24046.23 23387.48 172.13 o 5 2 0 9245.21 9098.17 138.31 o 6 2 0 10880.45 11048.82 167.79 o 7 2 0 1440.64 1610.04 115.40 o 8 2 0 258.63 292.52 125.30 o 9 2 0 2008.15 1988.34 156.04 o 10 2 0 2924.46 2430.48 182.00 o 1 3 0 5996.28 6904.17 72.53 o 2 3 0 118036.96 119156.02 319.81 o 3 3 0 12681.91 12604.59 125.72 o 4 3 0 22835.86 23035.53 182.85 o 5 3 0 1291.58 1357.71 92.07 o 6 3 0 3319.12 3265.41 115.48 o 7 3 0 2838.28 2801.03 131.88 o 8 3 0 9120.00 8425.47 202.66 o 9 3 0 902.93 729.45 152.98 o 10 3 0 49.77 0.43 162.02 o 0 4 0 134.60 167.65 54.44 o 1 4 0 46558.04 47446.13 193.05 o 2 4 0 83.50 196.16 51.85 o 3 4 0 9958.64 10516.81 128.08 o 4 4 0 1298.80 1531.14 85.16 o 5 4 0 28988.86 28875.80 235.68 o 6 4 0 88.01 79.07 105.42 o 7 4 0 2414.15 2492.83 132.73 o 8 4 0 92.66 255.78 132.21 o 9 4 0 4497.84 4113.78 185.54 o 10 4 0 142.30 227.70 167.64 o 1 5 0 217.32 222.53 46.67 o 2 5 0 55310.66 59017.73 259.81 o 3 5 0 2994.81 3081.58 90.42 o 4 5 0 12420.09 12793.85 163.66 o 5 5 0 33.74 0.00 94.19 o 6 5 0 4071.41 4198.07 139.29 o 7 5 0 1857.88 1918.38 142.65 o 8 5 0 8901.44 8444.61 219.95 o 9 5 0 93.73 0.00 157.27 o 10 5 0 111.54 395.33 170.66 o 0 6 0 15163.30 15620.96 172.82 o 1 6 0 35929.46 36964.80 211.85 o 2 6 0 6280.26 7244.14 117.85 o 3 6 0 6246.61 6107.12 126.04 o 4 6 0 3969.57 4181.64 117.68 o 5 6 0 15552.89 15451.00 204.06 o 6 6 0 5745.99 5591.12 167.91 o 7 6 0 853.40 837.06 139.15 o 8 6 0 118.38 374.60 141.72 o 9 6 0 2453.71 2804.61 233.86 o 10 6 0 937.86 878.95 185.82 o 1 7 0 16350.89 16301.87 164.87 o 2 7 0 11529.03 12045.34 154.08 o 3 7 0 32848.74 33710.04 254.87 o 4 7 0 316.79 457.59 97.22 o 5 7 0 120.86 133.94 107.58 o 6 7 0 1050.25 1235.15 134.41 o 7 7 0 10995.12 10794.46 232.64 o 8 7 0 3105.29 2961.19 183.32 o 9 7 0 1530.84 1504.88 178.93 o 0 8 0 29773.46 28812.88 270.44 o 1 8 0 2136.77 1894.32 86.05 o 2 8 0 3211.73 3204.28 99.05 o 3 8 0 481.85 510.76 91.61 o 4 8 0 8538.46 8288.79 167.64 o 5 8 0 181.15 120.98 116.66 o 6 8 0 8063.37 7937.16 203.48 o 7 8 0 456.59 416.97 151.67 o 8 8 0 36.78 6.48 155.11 o 9 8 0 19.39 0.43 174.98 o 1 9 0 18263.50 18409.72 201.26 o 2 9 0 346.62 504.69 85.99 o 3 9 0 18757.45 19158.89 226.81 o 4 9 0 1492.20 1565.98 118.43 o 5 9 0 3.51 186.65 117.95 o 6 9 0 12.91 47.53 136.53 o 7 9 0 6823.75 6999.70 217.23 o 8 9 0 72.07 363.79 162.45 o 9 9 0 1410.01 1632.74 191.45 o 0 10 0 18947.08 17356.77 256.83 o 1 10 0 2827.79 1992.16 112.43 o 2 10 0 696.93 513.81 97.23 o 3 10 0 281.24 425.17 102.40 o 4 10 0 7129.09 6871.78 167.52 o 5 10 0 4536.41 4640.27 182.53 o 6 10 0 5225.50 5381.26 199.85 o 7 10 0 144.68 98.51 154.68 o 8 10 0 31.75 0.43 168.07 o 1 11 0 3835.27 3726.09 145.76 o 2 11 0 7916.92 6786.10 168.00 o 3 11 0 6520.75 6093.21 159.27 o 4 11 0 4114.02 3852.22 158.29 o 5 11 0 25.91 0.00 136.53 o 6 11 0 718.70 1071.22 149.08 o 7 11 0 961.25 1140.84 168.53 o 8 11 0 2322.37 2536.88 198.84 o 0 12 0 1482.90 1396.49 161.22 o 1 12 0 8848.03 7307.51 179.71 o 2 12 0 6.37 0.00 106.72 o 3 12 0 585.50 603.66 122.29 o 4 12 0 312.07 345.23 131.35 o 5 12 0 5620.80 5577.88 186.88 o 6 12 0 161.72 121.41 156.41 o 7 12 0 512.04 472.71 172.84 o 1 13 0 51.39 62.65 112.77 o 2 13 0 9494.90 9942.19 226.04 o 3 13 0 17.87 0.00 125.29 o 4 13 0 2564.71 2476.20 162.11 o 5 13 0 17.59 31.11 146.03 o 6 13 0 1593.48 1657.45 180.66 o 0 14 0 2357.96 2551.76 197.99 o 1 14 0 5276.56 4714.54 161.35 o 2 14 0 500.61 176.30 133.95 o 3 14 0 62.13 45.80 130.91 o 4 14 0 735.84 719.47 150.38 o 5 14 0 3172.28 3045.77 185.04 o 1 15 0 294.22 268.32 128.33 o 2 15 0 1759.89 1482.05 152.14 o 3 15 0 1820.15 1679.15 162.51 o 4 15 0 492.89 553.08 152.96 o 0 16 0 2631.98 2910.56 229.11 o 1 16 0 688.83 683.17 141.30 o 2 16 0 395.54 383.69 141.72 o 1 0 1 87097.54 80051.23 156.26 o 2 0 1 806.32 1177.79 36.32 o 3 0 1 104.63 133.08 42.78 o 4 0 1 3639.21 3818.70 79.64 o 5 0 1 31579.67 30248.00 217.81 o 6 0 1 2723.96 2623.17 106.81 o 7 0 1 1860.09 1746.41 111.53 o 8 0 1 3567.70 3195.75 139.25 o 9 0 1 2526.80 2368.15 156.06 o 10 0 1 93.52 159.00 157.27 o -10 1 1 130.47 0.43 158.13 o -9 1 1 2076.29 2108.54 154.75 o -8 1 1 5607.80 4985.17 155.76 o -7 1 1 977.88 1033.75 107.61 o -6 1 1 8178.45 8529.93 161.15 o -5 1 1 27889.01 28609.04 220.98 o -4 1 1 10626.56 11626.05 130.71 o -3 1 1 13571.77 15042.90 121.56 o -2 1 1 16610.05 19806.07 112.23 o -1 1 1 44336.97 49944.43 143.75 o 0 1 1 1564.40 1769.79 23.41 o 1 1 1 44783.80 42869.38 126.83 o 2 1 1 15673.34 16523.50 99.00 o 3 1 1 12703.31 12513.96 107.12 o 4 1 1 10416.58 10320.54 118.97 o 5 1 1 27352.22 25394.39 201.72 o 6 1 1 8451.13 7753.44 150.77 o 7 1 1 1161.70 1209.28 105.89 o 8 1 1 5804.79 4827.06 170.91 o 9 1 1 1941.29 1846.54 153.88 o 10 1 1 157.59 159.43 159.00 o -10 2 1 981.03 716.05 168.97 o -9 2 1 2050.09 1703.07 155.61 o -8 2 1 2772.77 2467.43 143.11 o -7 2 1 4354.08 4090.92 135.83 o -6 2 1 5474.14 5517.10 123.79 o -5 2 1 15834.93 15457.77 170.38 o -4 2 1 10625.32 11165.50 129.38 o -3 2 1 28556.39 29638.11 169.99 o -2 2 1 6378.09 7776.14 85.98 o -1 2 1 14140.77 16661.27 93.47 o 0 2 1 30769.50 34361.03 114.25 o 1 2 1 15731.87 16775.63 89.67 o 2 2 1 6959.73 7469.95 79.93 o 3 2 1 25778.72 25945.55 157.00 o 4 2 1 12203.67 12252.40 132.08 o 5 2 1 15516.96 14608.46 163.41 o 6 2 1 5227.10 5087.34 122.04 o 7 2 1 4620.03 4422.18 136.27 o 8 2 1 2830.90 2596.74 142.68 o 9 2 1 1947.65 1937.31 153.88 o 10 2 1 1114.23 1352.63 163.35 o -10 3 1 972.30 1015.09 169.83 o -9 3 1 1688.10 1698.17 157.76 o -8 3 1 1942.03 1596.76 144.81 o -7 3 1 6059.01 6320.26 151.04 o -6 3 1 6450.73 6259.29 148.93 o -5 3 1 4961.52 5225.20 124.22 o -4 3 1 11759.42 12298.12 144.61 o -3 3 1 50741.61 52100.02 240.50 o -2 3 1 9982.79 10242.97 122.67 o -1 3 1 7407.32 8345.19 79.13 o 0 3 1 2085.69 1845.48 42.42 o 1 3 1 8145.38 8254.25 74.83 o 2 3 1 9873.12 9845.98 100.91 o 3 3 1 50048.33 50066.45 235.09 o 4 3 1 11121.17 11297.03 138.93 o 5 3 1 5488.26 5567.35 124.25 o 6 3 1 6628.07 6494.73 135.08 o 7 3 1 6010.45 5535.56 160.99 o 8 3 1 1937.48 1826.29 143.08 o 9 3 1 1446.85 1387.76 156.89 o 10 3 1 1011.18 792.55 171.13 o -10 4 1 2343.77 2137.95 185.87 o -9 4 1 810.35 957.16 158.59 o -8 4 1 1470.50 1631.14 146.95 o -7 4 1 4663.01 4715.29 151.41 o -6 4 1 11090.38 11387.48 184.24 o -5 4 1 788.85 1021.65 92.92 o -4 4 1 12400.44 12375.02 151.98 o -3 4 1 20226.29 22527.71 174.52 o -2 4 1 3819.63 4374.75 84.00 o -1 4 1 11963.22 13469.91 109.33 o 0 4 1 16423.86 17106.02 117.60 o 1 4 1 13759.61 13836.79 105.97 o 2 4 1 3968.83 4184.58 75.35 o 3 4 1 20720.92 21880.19 173.25 o 4 4 1 13735.50 13566.98 155.11 o 5 4 1 668.19 633.53 94.64 o 6 4 1 11309.76 11220.89 183.39 o 7 4 1 5235.87 5228.72 151.00 o 8 4 1 1506.95 1431.47 146.95 o 9 4 1 891.49 937.30 156.87 o 10 4 1 2421.14 2135.39 185.87 o -10 5 1 1055.08 1232.90 181.93 o -9 5 1 954.72 958.05 164.21 o -8 5 1 681.61 837.45 143.90 o -7 5 1 9578.61 9258.74 204.87 o -6 5 1 6001.70 5834.72 160.14 o -5 5 1 1123.61 1303.98 104.60 o -4 5 1 10914.08 11066.91 155.32 o -3 5 1 27912.60 29692.42 197.24 o -2 5 1 3032.21 3299.43 86.54 o -1 5 1 10340.88 11155.78 115.59 o 0 5 1 37337.66 39468.16 194.24 o 1 5 1 9765.67 10192.98 111.21 o 2 5 1 3896.30 4253.69 92.21 o 3 5 1 27249.81 27483.95 201.55 o 4 5 1 10138.63 10159.80 149.63 o 5 5 1 853.60 962.45 102.42 o 6 5 1 6463.63 6233.75 152.80 o 7 5 1 9007.71 8201.53 194.88 o 8 5 1 557.70 416.12 146.48 o 9 5 1 876.02 939.89 160.75 o 10 5 1 1067.90 808.54 183.66 o -10 6 1 1324.36 1003.05 192.75 o -9 6 1 810.30 1057.84 164.21 o -8 6 1 1695.67 1396.93 162.95 o -7 6 1 2669.64 2842.66 153.91 o -6 6 1 4515.40 4775.88 150.98 o -5 6 1 4737.30 5011.01 145.38 o -4 6 1 11236.23 11495.11 167.87 o -3 6 1 9013.61 8867.48 138.75 o -2 6 1 14558.82 15056.95 153.93 o -1 6 1 14623.33 15540.56 146.19 o 0 6 1 15797.97 14256.97 141.08 o 1 6 1 16020.28 14985.31 137.58 o 2 6 1 14383.22 14491.42 153.05 o 3 6 1 9738.74 9550.97 139.66 o 4 6 1 11340.99 11078.67 165.27 o 5 6 1 5064.82 5533.83 140.64 o 6 6 1 5281.42 5425.52 163.99 o 7 6 1 2584.76 2614.75 152.61 o 8 6 1 1791.36 1973.99 160.79 o 9 6 1 880.16 795.12 168.53 o 10 6 1 1353.90 1268.41 190.15 o -9 7 1 475.66 416.11 169.38 o -8 7 1 3207.63 3308.01 188.08 o -7 7 1 3187.78 3626.43 169.50 o -6 7 1 4452.15 4574.82 169.13 o -5 7 1 2516.30 2799.17 128.85 o -4 7 1 5370.90 5371.59 133.74 o -3 7 1 4394.43 4296.63 110.35 o -2 7 1 16591.04 16882.73 176.12 o -1 7 1 6100.60 6845.10 120.85 o 0 7 1 4596.27 3927.26 98.70 o 1 7 1 5781.62 6550.98 123.00 o 2 7 1 18552.56 16668.87 167.55 o 3 7 1 3959.94 3869.34 107.30 o 4 7 1 4830.53 4704.24 132.85 o 5 7 1 2874.05 3074.05 132.75 o 6 7 1 4619.22 5703.21 206.78 o 7 7 1 3076.10 3240.66 167.76 o 8 7 1 3023.30 3006.52 179.42 o 9 7 1 459.50 571.66 167.22 o -9 8 1 1258.55 1593.38 183.67 o -8 8 1 2060.73 2203.58 180.68 o -7 8 1 1051.97 1126.20 159.90 o -6 8 1 3307.91 3769.80 159.56 o -5 8 1 10157.52 12271.60 245.23 o -4 8 1 3805.70 3803.41 128.90 o -3 8 1 1506.49 1419.99 98.56 o -2 8 1 18608.26 19261.91 198.74 o -1 8 1 13947.38 13683.70 169.37 o 0 8 1 1616.39 1419.72 79.98 o 1 8 1 14628.54 12471.27 156.81 o 2 8 1 17968.87 17757.59 196.52 o 3 8 1 1808.45 1954.46 99.86 o 4 8 1 3647.31 3432.12 127.60 o 5 8 1 10499.88 10617.07 201.06 o 6 8 1 3230.65 3510.72 162.15 o 7 8 1 825.85 1028.48 149.52 o 8 8 1 1979.01 1679.67 178.08 o 9 8 1 1220.44 1311.17 184.96 o -9 9 1 447.43 464.06 187.96 o -8 9 1 2444.31 2920.01 184.15 o -7 9 1 492.03 504.26 152.53 o -6 9 1 2276.13 2548.78 155.62 o -5 9 1 4829.54 4877.55 163.96 o -4 9 1 4118.51 3865.73 157.88 o -3 9 1 396.25 456.73 98.52 o -2 9 1 10533.39 10587.58 171.24 o -1 9 1 5603.65 4833.70 127.69 o 0 9 1 977.77 917.98 82.55 o 1 9 1 4787.68 4711.66 135.45 o 2 9 1 11318.53 11642.62 186.02 o 3 9 1 563.27 622.26 98.96 o 4 9 1 4433.13 4233.35 138.00 o 5 9 1 5053.60 5172.03 163.53 o 6 9 1 2338.90 2367.69 162.54 o 7 9 1 638.81 870.27 152.97 o 8 9 1 2410.53 2633.83 182.85 o 9 9 1 558.44 509.88 184.07 o -8 10 1 653.56 808.04 175.87 o -7 10 1 403.90 686.16 154.69 o -6 10 1 1704.22 1904.37 158.63 o -5 10 1 7730.44 8196.60 193.06 o -4 10 1 3852.22 4214.62 164.35 o -3 10 1 1466.75 1346.39 113.24 o -2 10 1 5354.04 5485.28 152.75 o -1 10 1 5930.40 5420.71 124.65 o 0 10 1 2888.97 2843.24 105.51 o 1 10 1 6045.44 5090.21 138.51 o 2 10 1 4526.25 3974.95 118.54 o 3 10 1 1571.03 1728.96 113.25 o 4 10 1 4144.93 4094.28 146.19 o 5 10 1 7535.27 7290.23 199.55 o 6 10 1 1306.00 1566.66 154.29 o 7 10 1 368.30 581.15 154.69 o 8 10 1 715.30 805.46 174.14 o -8 11 1 487.18 753.14 175.43 o -7 11 1 1328.31 1506.55 170.71 o -6 11 1 1359.87 1343.22 160.77 o -5 11 1 1747.58 1965.34 151.71 o -4 11 1 4136.00 4124.27 159.16 o -3 11 1 5028.82 4503.55 146.66 o -2 11 1 3869.87 3405.97 127.16 o -1 11 1 3893.01 3244.75 123.27 o 0 11 1 3299.95 2931.15 116.33 o 1 11 1 3861.77 3496.44 124.13 o 2 11 1 3898.65 3706.15 153.97 o 3 11 1 5069.39 4413.61 158.34 o 4 11 1 4114.39 4071.92 156.99 o 5 11 1 1686.67 1582.36 154.30 o 6 11 1 1317.08 1394.20 160.77 o 7 11 1 1360.61 1389.87 171.14 o 8 11 1 513.72 737.58 180.62 o -7 12 1 963.85 1311.10 178.47 o -6 12 1 1769.39 1832.15 171.16 o -5 12 1 536.61 568.65 143.89 o -4 12 1 3413.08 3504.57 153.07 o -3 12 1 3927.18 3962.68 153.09 o -2 12 1 1388.17 1176.02 118.86 o -1 12 1 1658.12 1441.50 118.43 o 0 12 1 8392.82 7085.91 173.20 o 1 12 1 1857.69 1486.96 118.87 o 2 12 1 1278.97 1229.15 115.39 o 3 12 1 3768.80 3653.32 148.76 o 4 12 1 3734.12 3443.43 160.00 o 5 12 1 546.32 586.80 143.89 o 6 12 1 1643.67 1823.89 170.29 o 7 12 1 1131.45 1348.30 179.34 o -6 13 1 782.49 762.26 171.12 o -5 13 1 25.37 0.43 144.31 o -4 13 1 1329.66 1139.22 148.24 o -3 13 1 4461.91 4256.60 164.78 o -2 13 1 328.06 453.69 117.96 o -1 13 1 2453.65 2135.59 131.42 o 0 13 1 3500.45 2847.46 137.94 o 1 13 1 2235.65 1827.69 130.98 o 2 13 1 336.70 77.34 122.71 o 3 13 1 4621.60 4450.96 161.76 o 4 13 1 960.84 982.69 141.31 o 5 13 1 38.33 0.43 149.06 o 6 13 1 793.35 728.55 168.96 o -5 14 1 464.39 503.82 159.44 o -4 14 1 1267.03 1261.49 155.15 o -3 14 1 1495.51 1711.91 146.08 o -2 14 1 998.27 786.51 133.10 o -1 14 1 1885.33 1883.68 137.45 o 0 14 1 4808.90 4252.56 160.47 o 1 14 1 1962.59 1704.76 137.45 o 2 14 1 852.17 847.84 131.80 o 3 14 1 1440.06 1240.37 144.78 o 4 14 1 1430.09 1408.04 154.29 o 5 14 1 389.56 618.74 153.82 o -4 15 1 888.20 1037.54 156.43 o -3 15 1 1225.80 889.38 159.47 o -2 15 1 1522.44 1509.20 149.54 o -1 15 1 1365.13 1392.90 136.57 o 0 15 1 996.79 716.49 135.69 o 1 15 1 1118.68 1058.34 141.31 o 2 15 1 1690.56 1652.32 149.11 o 3 15 1 1361.18 1520.38 153.42 o 4 15 1 776.57 812.81 155.13 o -2 16 1 800.63 933.38 146.49 o -1 16 1 1223.80 1146.08 146.93 o 0 16 1 481.61 330.98 140.00 o 1 16 1 1241.07 1266.22 145.64 o 2 16 1 758.46 549.65 148.65 o 0 0 2 21324.10 22617.30 140.96 o 1 0 2 35614.01 33558.74 111.93 o 2 0 2 18.26 46.66 32.84 o 3 0 2 13541.34 14587.19 116.30 o 4 0 2 75.71 20.74 57.46 o 5 0 2 245.11 326.66 74.75 o 6 0 2 737.29 821.09 93.35 o 7 0 2 10555.19 9063.01 181.57 o 8 0 2 90.35 22.90 121.84 o 9 0 2 2639.36 2455.96 153.90 o 10 0 2 302.41 328.81 155.98 o -10 1 2 3251.64 3072.67 179.42 o -9 1 2 668.99 712.99 144.33 o -8 1 2 92.52 110.18 118.38 o -7 1 2 2067.95 2092.78 115.42 o -6 1 2 10481.91 9806.23 166.91 o -5 1 2 2963.07 3046.81 94.29 o -4 1 2 19223.73 20501.60 167.39 o -3 1 2 12039.71 13913.63 120.97 o -2 1 2 5049.49 5934.66 73.32 o -1 1 2 15694.55 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