Crystallography Open Database

Information card for entry 4320633

4320632 << 4320633 >> 4320634

Preview

Coordinates	4320633.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[Cobalt(III) sepulcherate] heptacyano-(2-peroxo tungsten(VI) tetra-hydrate
Formula	C21 H32 Co N13 O6 W
Calculated formula	C21 H32 Co N13 O6 W
Title of publication	Reaction of [Os(en)2O2]2+ with Photolyzed [Mo(CN)8]4- in Water
Authors of publication	R. Kent Murmann; Charles L. Barnes
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	6514 - 6517
a	14.2689 ± 0.0014 Å
b	13.2323 ± 0.0013 Å
c	15.2384 ± 0.0016 Å
α	90°
β	103.397 ± 0.002°
γ	90°
Cell volume	2798.9 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.038
Weighted residual factors for significantly intense reflections	0.0906
Weighted residual factors for all reflections included in the refinement	0.0957
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179309 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/06.	4320633.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320633.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320633.cif
17829	2011-04-10	../uploads/cif-deposit/cod/cif Adding structures of 4320633 via cif-deposit CGI script.	4320633.cif