Crystallography Open Database

Information card for entry 4320707

4320706 << 4320707 >> 4320708

Preview

Coordinates	4320707.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Al2 Co3 H54 K12 O108 W22
Calculated formula	Al2 Co2.92 K12 O107.96 W22.08
Title of publication	Formation, Isomerization, and Derivatization of Keggin Tungstoaluminates
Authors of publication	Jennifer J. Cowan; Alan J. Bailey; Robert A. Heintz; Bao T. Do; Kenneth I. Hardcastle; Craig L. Hill; Ira A. Weinstock
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	6666 - 6675
a	15.6315 ± 0.0016 Å
b	15.6328 ± 0.0016 Å
c	15.6522 ± 0.0016 Å
α	90.024 ± 0.002°
β	60.011 ± 0.002°
γ	60.039 ± 0.002°
Cell volume	2706 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0896
Residual factor for significantly intense reflections	0.0616
Weighted residual factors for significantly intense reflections	0.1317
Weighted residual factors for all reflections included in the refinement	0.1375
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4320707.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320707.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320707.cif
17903	2011-04-11	../uploads/cif-deposit/cod/cif Adding structures of 4320707 via cif-deposit CGI script.	4320707.cif