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Information card for entry 4320723
Preview
| Coordinates | 4320723.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C40 H52 Cl2 Cu4 N16 O28 |
|---|---|
| Calculated formula | C40 H52 Cl2 Cu4 N16 O28 |
| Title of publication | Two Polymeric Compounds Built from Mononuclear and Tetrameric Squarate-Copper(II) Complexes by Deprotonation of 3,3-Bis(2-imidazolyl)propionic Acid (HBIP). Synthesis, Crystal Structure, and Magnetic Characterization of [Cu(HBIP)(BIP)](C4O4)1/2.2H2O and [{Cu(BIP)(OH2)}4(μ-C4O4)](ClO4)2.4H2O |
| Authors of publication | Youness Akhriff; Juan Server-Carrió; Amparo Sancho; Julia García-Lozano; Emilio Escrivá; Lucía Soto |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2001 |
| Journal volume | 40 |
| Pages of publication | 6832 - 6840 |
| a | 8.01 ± 0.001 Å |
| b | 13.073 ± 0.001 Å |
| c | 14.561 ± 0.001 Å |
| α | 72.13 ± 0.01° |
| β | 80.14 ± 0.01° |
| γ | 84.02 ± 0.01° |
| Cell volume | 1427.6 ± 0.2 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0549 |
| Residual factor for significantly intense reflections | 0.0456 |
| Weighted residual factors for significantly intense reflections | 0.1214 |
| Weighted residual factors for all reflections included in the refinement | 0.1331 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179310 (current) | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/07. |
4320723.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4320723.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4320723.cif |
| 17919 | 2011-04-11 | ../uploads/cif-deposit/cod/cif Adding structures of 4320723 via cif-deposit CGI script. |
4320723.cif |
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Users of the data should acknowledge the original authors of the
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