Crystallography Open Database

Information card for entry 4321104

Preview

Coordinates	4321104.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H227 Mo57 N21 O283 V12
Calculated formula	Mo57 N6 O275 V12
Title of publication	(NH4)15[H3Mo57V6(NO)6O189(H2O)12(VO)6].~60H2O: New Nanocompound Obtained by Chemical Embellishment of {M57V6}
Authors of publication	Wenbin Yang; Xiang Lin; Canzhong Lu; Honghui Zhuang; Jinshun Huang
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	2706 - 2707
a	23.612 ± 0.003 Å
b	23.612 ± 0.003 Å
c	26.859 ± 0.005 Å
α	90°
β	90°
γ	120°
Cell volume	12968 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	194
Hermann-Mauguin space group symbol	P 63/m m c
Hall space group symbol	-P 6c 2c
Residual factor for all reflections	0.0844
Residual factor for significantly intense reflections	0.0546
Weighted residual factors for significantly intense reflections	0.1699
Weighted residual factors for all reflections included in the refinement	0.1877
Goodness-of-fit parameter for all reflections included in the refinement	0.938
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179314 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/11.	4321104.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321104.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321104.cif
18451	2011-04-29	../uploads/cif-deposit/cod/cif Adding structures of 4321104 via cif-deposit CGI script.	4321104.cif