Crystallography Open Database

Information card for entry 4321172

Preview

Coordinates	4321172.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H58 N10 Ni O10
Calculated formula	C50 H46 N10 Ni O10
Title of publication	Synthesis, Characterization, and Spontaneous Resolution of Chiral Nickel(II) Complexes with the Tripod Ligand Tris[2-(((2-phenylimidazol-4-yl)methylidene)amino)ethyl]amine
Authors of publication	Ikuko Katsuki; Naohide Matsumoto; Masaaki Kojima
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	3350 - 3354
a	14.191 ± 0.005 Å
b	16.048 ± 0.004 Å
c	13.692 ± 0.004 Å
α	115.25 ± 0.02°
β	111.07 ± 0.03°
γ	64.75 ± 0.02°
Cell volume	2490 ± 1.4 Å³
Cell temperature	293.2 K
Ambient diffraction temperature	293.2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0874
Residual factor for significantly intense reflections	0.0874
Weighted residual factors for significantly intense reflections	0.0862
Weighted residual factors for all reflections included in the refinement	0.0862
Goodness-of-fit parameter for all reflections included in the refinement	2.615
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4321172.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321172.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321172.cif
18521	2011-05-01	../uploads/cif-deposit/cod/cif Adding structures of 4321172 via cif-deposit CGI script.	4321172.cif