Crystallography Open Database

Information card for entry 4321177

Preview

Coordinates	4321177.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C240.5 H338 Eu18 O51
Calculated formula	C240.5 H319.5 Eu18 O51
Title of publication	Reactivity of "Eu(OiPr)2" with Phenols: Formation of Linear Eu3, Square Pyramidal Eu5, Cubic Eu8, and Capped Cubic Eu9 Polymetallic Europium Complexes
Authors of publication	William J. Evans; Michael A. Greci; Joseph W. Ziller
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	3213 - 3220
a	14.9535 ± 0.0007 Å
b	28.3557 ± 0.0013 Å
c	30.0169 ± 0.0014 Å
α	89.046 ± 0.001°
β	86.618 ± 0.001°
γ	80.75 ± 0.001°
Cell volume	12540 ± 1 Å³
Cell temperature	158 ± 2 K
Ambient diffraction temperature	158 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.154
Residual factor for significantly intense reflections	0.0941
Weighted residual factors for significantly intense reflections	0.137
Weighted residual factors for all reflections included in the refinement	0.1572
Goodness-of-fit parameter for all reflections included in the refinement	1.184
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4321177.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321177.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321177.cif
18526	2011-05-01	../uploads/cif-deposit/cod/cif Adding structures of 4321177 via cif-deposit CGI script.	4321177.cif