Crystallography Open Database

Information card for entry 4321829

Preview

Coordinates	4321829.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H30 Ag3 N S6 W2
Calculated formula	C21 H30 Ag3 N S6 W2
Title of publication	Aggregation of the Half-Sandwich Trisulfido Complex of Tungsten with Silver Ions: Synthesis of a Cyanide-Bridged Helical Polymer {[(η5-C5Me5)WS3]2Ag3(CN)}∞and a Cyclic Cluster [(η5-C5Me5)WS3Ag]4
Authors of publication	Jian-Ping Lang; Kazuyuki Tatsumi
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	1364 - 1367
a	15.415 ± 0.005 Å
b	9.616 ± 0.006 Å
c	21.659 ± 0.004 Å
α	90°
β	109.91 ± 0.02°
γ	90°
Cell volume	3019 ± 2 Å³
Cell temperature	296.2 K
Ambient diffraction temperature	296.2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0
Residual factor for significantly intense reflections	0
Weighted residual factors for significantly intense reflections	0
Weighted residual factors for all reflections included in the refinement	0.0542
Goodness-of-fit parameter for all reflections included in the refinement	1.526
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4321829.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321829.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321829.cif
19640	2011-05-22	../uploads/cif-deposit/cod/cif Adding structures of 4321829 via cif-deposit CGI script.	4321829.cif