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Information card for entry 4321950
Preview
Coordinates | 4321950.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25.5 H23 Cl I2 P2 Pd S |
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Calculated formula | C25.5 H22 Cl I2 P2 Pd S |
Title of publication | Kinetic and Mechanistic Aspects of Sulfur Recovery from Pd~2~I~2~(μ-S)(μ-dpm)~2~ Using I2 and Structures of Pd(II) Complexes with the Chelated Monosulfide of dpm |
Authors of publication | Terrance Y. H. Wong; Steven J. Rettig; Brian R. James |
Journal of publication | Inorganic Chemistry |
Year of publication | 1999 |
Journal volume | 38 |
Pages of publication | 2143 - 2149 |
a | 9.378 ± 0.002 Å |
b | 14.231 ± 0.003 Å |
c | 21.049 ± 0.002 Å |
α | 90° |
β | 91.603 ± 0.015° |
γ | 90° |
Cell volume | 2808.1 ± 0.9 Å3 |
Cell temperature | 294.2 K |
Ambient diffraction temperature | 294.2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for significantly intense reflections | 0.035 |
Weighted residual factors for all reflections included in the refinement | 0.028 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.32 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4321950.cif |
130086 | 2015-01-23 | cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ | xargs -i sh -c 'cif_fix_values {} \ | cif_filter --add-cif-header {} \ | sponge {}' |
4321950.cif |
120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4321950.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4321950.cif |
19814 | 2011-05-26 | ../uploads/cif-deposit/cod/cif Adding structures of 4321950 via cif-deposit CGI script. |
4321950.cif |
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