Crystallography Open Database

Information card for entry 4322027

4322026 << 4322027 >> 4322028

Preview

Coordinates	4322027.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H29 Cl3 N2 O6 P2 W
Calculated formula	C23 H29 Cl3 N2 O6 P2 W
Title of publication	Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1
Authors of publication	Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	2489 - 2496
a	10.068 ± 0.001 Å
b	10.756 ± 0.001 Å
c	14.323 ± 0.002 Å
α	98.64 ± 0.01°
β	96.33 ± 0.009°
γ	96.472 ± 0.009°
Cell volume	1510.9 ± 0.3 Å³
Cell temperature	293.2 K
Ambient diffraction temperature	293.2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.032
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.0289
Weighted residual factors for all reflections included in the refinement	0.0289
Goodness-of-fit parameter for all reflections included in the refinement	2.014
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322027.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322027.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322027.cif
19916	2011-05-30	../uploads/cif-deposit/cod/cif Adding structures of 4322027 via cif-deposit CGI script.	4322027.cif