Crystallography Open Database

Information card for entry 4322040

4322039 << 4322040 >> 4322041

Preview

Coordinates	4322040.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Bi2 H50 K3 Na7 O95 W20 Zn2
Calculated formula	Bi2 K3 Na7 O95 W20 Zn2
Title of publication	Heteropolymetalate Clusters of the Subvalent Main Group Elements BiIII and SbIII
Authors of publication	Ina Loose; Elisabeth Droste; Michael Bösing; Heinrich Pohlmann; Michael H. Dickman; Cristina Rosu; Michael T. Pope; Bernt Krebs
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	2688 - 2694
a	12.852 ± 0.003 Å
b	17.512 ± 0.004 Å
c	18.908 ± 0.004 Å
α	90°
β	91.99 ± 0.03°
γ	90°
Cell volume	4252.9 ± 1.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1193
Residual factor for significantly intense reflections	0.0856
Weighted residual factors for significantly intense reflections	0.2088
Weighted residual factors for all reflections included in the refinement	0.2332
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322040.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322040.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322040.cif
19930	2011-05-31	../uploads/cif-deposit/cod/cif Adding structures of 4322040 via cif-deposit CGI script.	4322040.cif