Crystallography Open Database

Information card for entry 4322145

Preview

Coordinates	4322145.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H27 P Re S3
Calculated formula	C29 H27 P Re S3
Title of publication	Synthesis and Structural Characterization of Novel Terminal and Bridging Re(V)-Sulfido Complexes
Authors of publication	Josemon Jacob; Ilia A. Guzei; James H. Espenson
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	3266 - 3267
a	9.2936 ± 0.0005 Å
b	22.2088 ± 0.0012 Å
c	13.0576 ± 0.0007 Å
α	90°
β	91.237 ± 0.001°
γ	90°
Cell volume	2694.5 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0408
Residual factor for significantly intense reflections	0.0246
Weighted residual factors for significantly intense reflections	0.0416
Weighted residual factors for all reflections included in the refinement	0.0436
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179324 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/21.	4322145.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322145.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322145.cif
20394	2011-06-05	../uploads/cif-deposit/cod/cif Adding structures of 4322145 via cif-deposit CGI script.	4322145.cif