Crystallography Open Database

Information card for entry 4322191

Preview

Coordinates	4322191.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H57 Cl N4 Si3 U
Calculated formula	C24 H57 Cl N4 Si3 U
SMILES	[U]123(Cl)N([Si](C)(C)C(C)(C)C)CC[N]3(CCN1[Si](C)(C)C(C)(C)C)CCN2[Si](C)(C)C(C)(C)C
Title of publication	Complexes of Triamidoamines with the Early Actinides. Synthetic Routes to Monomeric Compounds of Tetravalent Uranium and Thorium Containing Halide and Amide Ligands
Authors of publication	Paul Roussel; Nathaniel W. Alcock; Rita Boaretto; Andrew J. Kingsley; Ian J. Munslow; Christopher J. Sanders; Peter Scott
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	3651 - 3656
a	22.7553 ± 0.001 Å
b	15.1678 ± 0.001 Å
c	22.7921 ± 0.001 Å
α	90°
β	116.69°
γ	90°
Cell volume	7028.5 ± 0.6 Å³
Cell temperature	210 ± 2 K
Ambient diffraction temperature	210 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0738
Residual factor for significantly intense reflections	0.0611
Weighted residual factors for significantly intense reflections	0.1574
Weighted residual factors for all reflections included in the refinement	0.1718
Goodness-of-fit parameter for all reflections included in the refinement	1.242
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179324 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/21.	4322191.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322191.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322191.cif
20450	2011-06-07	../uploads/cif-deposit/cod/cif Adding structures of 4322191 via cif-deposit CGI script.	4322191.cif