Crystallography Open Database

Information card for entry 4322413

Preview

Coordinates	4322413.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 F3 Fe N3 O2 Si4 Ti
Calculated formula	C32 H38 F3 Fe N3 O2 Si4 Ti
Title of publication	Synthesis and Reactivity of Early-Late Heterodinuclear Complexes Stabilized by a Trisilylsilane-Based Tripodal Amido Ligand
Authors of publication	Lutz H. Gade; Martin Schubart; Bernd Findeis; Sylvie Fabre; Izoldi Bezougli; Matthias Lutz; Ian J. Scowen; Mary McPartlin
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	5282 - 5294
a	19.903 ± 0.002 Å
b	10.572 ± 0.004 Å
c	19.111 ± 0.003 Å
α	90°
β	112.939 ± 0.009°
γ	90°
Cell volume	3703.2 ± 1.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.2591
Residual factor for significantly intense reflections	0.0974
Weighted residual factors for significantly intense reflections	0.1248
Weighted residual factors for all reflections included in the refinement	0.1574
Goodness-of-fit parameter for all reflections included in the refinement	0.922
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179327 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/24.	4322413.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322413.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322413.cif
20685	2011-06-12	../uploads/cif-deposit/cod/cif Adding structures of 4322413 via cif-deposit CGI script.	4322413.cif