Crystallography Open Database

Information card for entry 4322416

Preview

Coordinates	4322416.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	di-[(N,N'-ethylenebis(salicylideneiminato)nickel(ii)]-di-aquo-nickel(ii)perc hlorate
Formula	C32 H32 Cl2 N4 Ni3 O14
Calculated formula	C32 H32 Cl2 N4 Ni3 O14
Title of publication	Spectrophotometric Study of the Equilibria between Nickel(II) Schiff-Base Complexes and Alkaline Earth or Nickel(II) Cations in Acetonitrile Solution
Authors of publication	Laura Carbonaro; Mauro Isola; Piero La Pegna; Lucio Senatore; Fabio Marchetti
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	5519 - 5525
a	10.302 ± 0.0015 Å
b	21.818 ± 0.003 Å
c	17.796 ± 0.004 Å
α	90°
β	118.98 ± 0.02°
γ	90°
Cell volume	3499.1 ± 1.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1186
Residual factor for significantly intense reflections	0.065
Weighted residual factors for significantly intense reflections	0.1396
Weighted residual factors for all reflections included in the refinement	0.165
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179327 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/24.	4322416.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322416.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322416.cif
20688	2011-06-12	../uploads/cif-deposit/cod/cif Adding structures of 4322416 via cif-deposit CGI script.	4322416.cif