Crystallography Open Database

Information card for entry 4322493

Preview

Coordinates	4322493.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25.5 H19 Ag F3 O3 S
Calculated formula	C25.5 H15 Ag F3 O3 S
Title of publication	Mobility of Silver(I) Ions around the Propeller Ligand, Hexaphenylbenzene (HPB), in Silver(I) π-Complexes
Authors of publication	Gui Ling Ning; Megumu Munakata; Liang Ping Wu; Masahiko Maekawa; Yusaku Suenaga; Takayoshi Kuroda-Sowa; Kunihisa Sugimoto
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	5668 - 5673
a	18.2 ± 0.004 Å
b	16.831 ± 0.007 Å
c	16.244 ± 0.003 Å
α	90°
β	110.96 ± 0.02°
γ	90°
Cell volume	4647 ± 2 Å³
Cell temperature	296.2 K
Ambient diffraction temperature	296.2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0565
Residual factor for significantly intense reflections	0.0565
Weighted residual factors for significantly intense reflections	0.0673
Weighted residual factors for all reflections included in the refinement	0.0673
Goodness-of-fit parameter for all reflections included in the refinement	2.39
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322493.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322493.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322493.cif
20775	2011-06-13	../uploads/cif-deposit/cod/cif Adding structures of 4322493 via cif-deposit CGI script.	4322493.cif