Crystallography Open Database

Information card for entry 4322584

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Coordinates	4322584.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	{N,N'-di-3-ethoxysalicylidene-(R,S)(S,R)-1,2-diphenyl-1,2-ethanediamine} oxovanadium
Formula	C32 H32 N2 O6 V
Calculated formula	C32 H32 N2 O6 V
SMILES	[V]123(=O)Oc4c(OCC)cccc4C=[N]2[C@@H](c2ccccc2)[C@H]([N]3=Cc2cccc(OCC)c2O1)c1ccccc1.O
Title of publication	Thermal Dehydrogenation of Oxovanadium(IV) Complexes with Schiff Base Ligands Derived from meso-1,2-Diphenyl-1,2-ethanediamine in the Solid State
Authors of publication	Gakuse Hoshina; Masanobu Tsuchimoto; Shigeru Ohba; Kiyohiko Nakajima; Hidehiro Uekusa; Yuji Ohashi; Hiroyuki Ishida; Masaaki Kojima
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	142 - 145
a	16.528 ± 0.002 Å
b	11.031 ± 0.002 Å
c	17.189 ± 0.002 Å
α	90 ± 0°
β	112.482 ± 0.008°
γ	90 ± 0°
Cell volume	2895.7 ± 0.7 Å³
Cell temperature	298 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.061
Weighted residual factors for significantly intense reflections	0.049
Goodness-of-fit parameter for significantly intense reflections	1.28
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322584.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322584.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322584.cif
21446	2011-06-22	../uploads/cif-deposit/cod/cif Adding structures of 4322584 via cif-deposit CGI script.	4322584.cif