Crystallography Open Database

Information card for entry 4322950

Preview

Coordinates	4322950.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H140 Mo6 O66 S16 Sb
Calculated formula	C56 Mo6 O66 S16 Sb
Title of publication	Sulfur-Bridged Sandwich Cubane-Type Molybdenum-Antimony Cluster. Synthesis, X-ray Structure, and 121Sb Mössbauer Spectra of [(H2O)9Mo3S4SbS4Mo3(H2O)9](CH3C6H4SO3)8.24H2O
Authors of publication	Genta Sakane; Kouichi Hashimoto; Masashi Takahashi; Masuo Takeda; Takashi Shibahara
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	4231 - 4234
a	14.468 ± 0.003 Å
b	18.531 ± 0.005 Å
c	13.713 ± 0.006 Å
α	105.26 ± 0.02°
β	119.71 ± 0.01°
γ	72.48 ± 0.03°
Cell volume	3016.1 ± 1.7 Å³
Cell temperature	298.2 K
Ambient diffraction temperature	298.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0
Residual factor for significantly intense reflections	0
Weighted residual factors for significantly intense reflections	0
Weighted residual factors for all reflections included in the refinement	0.0747
Goodness-of-fit parameter for all reflections included in the refinement	1.332
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322950.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322950.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322950.cif
21899	2011-06-29	../uploads/cif-deposit/cod/cif Adding structures of 4322950 via cif-deposit CGI script.	4322950.cif