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Information card for entry 4323359
Preview
| Coordinates | 4323359.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C47 H54 B M N3 O7 P2 |
|---|---|
| Calculated formula | C47 H54 B Mn N2 O7 P2 |
| Title of publication | Aryldiazene, Aryldiazenido, and Hydrazine Complexes of Manganese. Preparation, Characterization, and X-ray Crystal Structures of [Mn(CO)3(4-CH3C6H4NNH){PPh(OEt)2}2]BF4 and [Mn(CO)3(NH2NH2){PPh(OEt)2}2]BPh4 Derivatives |
| Authors of publication | Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Emilio Bordignon; Fabio Busatto; Giancarlo Pelizzi |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 1997 |
| Journal volume | 36 |
| Pages of publication | 1296 - 1305 |
| a | 13.772 ± 0.003 Å |
| b | 14.951 ± 0.004 Å |
| c | 13.319 ± 0.003 Å |
| α | 104.47 ± 0.01° |
| β | 100.32 ± 0.01° |
| γ | 111.08 ± 0.01° |
| Cell volume | 2365.4 ± 1 Å3 |
| Cell temperature | 295 K |
| Ambient diffraction temperature | 295 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.094 |
| Residual factor for significantly intense reflections | 0.0511 |
| Weighted residual factors for all reflections | 0.173 |
| Goodness-of-fit parameter for all reflections | 1.024 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211332 (current) | 2018-10-05 | cif/ Fixing enumeration values for CIF data items _atom_sites_solution_* using cif_fix_values. Data item relocations and exclusion of CIF comment lines might have occurred due to the usage of cif_filter. |
4323359.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4323359.cif |
| 132089 | 2015-02-20 | cif/ (antanas@koala.ibt.lt) Replacing '_chemical_name_systematic' tag values consisting of '.....' with a single '?'. |
4323359.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4323359.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4323359.cif |
| 23387 | 2011-08-07 | ../uploads/cif-deposit/cod/cif Adding structures of 4323359 via cif-deposit CGI script. |
4323359.cif |
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