Crystallography Open Database

Information card for entry 4324111

Preview

Coordinates	4324111.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	SU-63
Formula	Ge21 O51
Calculated formula	Ge21 O51
Title of publication	Investigation of the GeO2-1,6-Diaminohexane-Water-Pyridine-HF Phase Diagram Leading to the Discovery of Two Novel Layered Germanates with Extra-Large Rings
Authors of publication	Bing Guo; Andrew K. Inge; Charlotte Bonneau; Junliang Sun; Kirsten E. Christensen; Zhong-Yong Yuan; Xiaodong Zou
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	201 - 207
a	28.794 ± 0.002 Å
b	28.794 ± 0.002 Å
c	20.603 ± 0.004 Å
α	90°
β	90°
γ	120°
Cell volume	14793 ± 3 Å³
Cell temperature	106 ± 2 K
Ambient diffraction temperature	106 ± 2 K
Number of distinct elements	2
Space group number	185
Hermann-Mauguin space group symbol	P 63 c m
Hall space group symbol	P 6c -2
Residual factor for all reflections	0.1112
Residual factor for significantly intense reflections	0.0851
Weighted residual factors for significantly intense reflections	0.2163
Weighted residual factors for all reflections included in the refinement	0.2422
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.908 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179344 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/41.	4324111.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324111.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4324111.cif
24402	2011-08-23	../uploads/cif-deposit/cod/cif Adding structures of 4324111 via cif-deposit CGI script.	4324111.cif