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Information card for entry 4324172
Preview
| Coordinates | 4324172.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H58 F4 N10 Si2 |
|---|---|
| Calculated formula | C36 H58 F4 N10 Si2 |
| SMILES | F[Si]12(F)[N]3=C(N=C(N(c4c(C(C)C)cccc4C(C)C)[Si]3(F)(F)[N]1=C(N=C(N2c1c(C(C)C)cccc1C(C)C)N(C)C)N(C)C)N(C)C)N(C)C |
| Title of publication | Neutral Pentacoordinate Silicon Fluorides Derived from Amidinate, Guanidinate, and Triazapentadienate Ligands and Base-Induced Disproportionation of Si2Cl6 to Stable Silylenes |
| Authors of publication | Rajendra S. Ghadwal; Kevin Pröpper; Birger Dittrich; Peter G. Jones; Herbert W. Roesky |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2011 |
| Journal volume | 50 |
| Pages of publication | 358 - 364 |
| a | 14.4012 ± 0.0003 Å |
| b | 14.4485 ± 0.0003 Å |
| c | 9.8332 ± 0.0002 Å |
| α | 90° |
| β | 101.97 ± 0.001° |
| γ | 90° |
| Cell volume | 2001.56 ± 0.07 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.0223 |
| Residual factor for significantly intense reflections | 0.0218 |
| Weighted residual factors for significantly intense reflections | 0.0555 |
| Weighted residual factors for all reflections included in the refinement | 0.0557 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179344 (current) | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/41. |
4324172.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4324172.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4324172.cif |
| 24463 | 2011-08-23 | ../uploads/cif-deposit/cod/cif Adding structures of 4324172 via cif-deposit CGI script. |
4324172.cif |
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