Crystallography Open Database

Information card for entry 4324424

Preview

Coordinates	4324424.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H40 Cl2 N12 Re2
Calculated formula	C24 H40 Cl2 N12 Re2
Title of publication	Tuning the Electrochemistry of Re26+ Species with Divergent Bicyclic Guanidinate Ligands and by Modification of Axial π Interactions
Authors of publication	Gina M. Chiarella; F. Albert Cotton; Carlos A. Murillo; Mark D. Young
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	1258 - 1264
a	9.679 ± 0.004 Å
b	9.679 ± 0.004 Å
c	15.448 ± 0.008 Å
α	90°
β	90°
γ	90°
Cell volume	1447.2 ± 1.1 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	5
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0714
Residual factor for significantly intense reflections	0.0599
Weighted residual factors for significantly intense reflections	0.1435
Weighted residual factors for all reflections included in the refinement	0.1482
Goodness-of-fit parameter for all reflections included in the refinement	1.915
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179347 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/44.	4324424.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324424.cif
41132	2012-03-12	../uploads/cif-deposit/cod/cif Adding structures of 4324424 via cif-deposit CGI script.	4324424.cif