Crystallography Open Database

Information card for entry 4325109

Preview

Coordinates	4325109.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	apx1122
Formula	C18 H29 Cl2 N O2 U
Calculated formula	C18 H29 Cl2 N O2 U
Title of publication	A General and Modular Synthesis of Monoimidouranium(IV) Dihalides
Authors of publication	Robert E. Jilek; Liam P. Spencer; David L. Kuiper; Brian L. Scott; Ursula J. Williams; James M. Kikkawa; Eric J. Schelter; James M. Boncella
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	4235 - 4237
a	12.75 ± 0.003 Å
b	12.635 ± 0.003 Å
c	13.145 ± 0.003 Å
α	90°
β	104.092 ± 0.002°
γ	90°
Cell volume	2053.9 ± 0.8 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0631
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.1048
Weighted residual factors for all reflections included in the refinement	0.1177
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179354 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/51.	4325109.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325109.cif
43561	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4325109 via cif-deposit CGI script.	4325109.cif