Crystallography Open Database

Information card for entry 4325240

Preview

Coordinates	4325240.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Uranium(IV) monoiodotetrakis(tetrahydrofuran)bistrimethylsilyloxide Triiodide
Formula	C22 H50 I4 O6 Si2 U
Calculated formula	C22 H25 I4 O6 Si2 U
Title of publication	Facile Reduction of a Uranyl(VI) β-Ketoiminate Complex to U(IV) Upon Oxo Silylation
Authors of publication	Jessie L. Brown; Charles C. Mokhtarzadeh; Jeremie M. Lever; Guang Wu; Trevor W. Hayton
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	5105 - 5112
a	9.519 ± 0.004 Å
b	12.725 ± 0.005 Å
c	16.355 ± 0.006 Å
α	89.944 ± 0.006°
β	74.313 ± 0.006°
γ	89.97 ± 0.006°
Cell volume	1907.3 ± 1.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0919
Residual factor for significantly intense reflections	0.0483
Weighted residual factors for significantly intense reflections	0.105
Weighted residual factors for all reflections included in the refinement	0.1224
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179355 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/52.	4325240.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325240.cif
43693	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4325240 via cif-deposit CGI script.	4325240.cif