Crystallography Open Database

Information card for entry 4325448

Preview

Coordinates	4325448.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H154 F7 Ga10 O6 Rh2 S2
Calculated formula	C108 H154 F7 Ga10 O6 Rh2 S2
Title of publication	Homoleptic Hexa and Penta Gallylene Coordinated Complexes of Molybdenum and Rhodium
Authors of publication	Timo Bollermann; Thomas Cadenbach; Christian Gemel; Kerstin Freitag; Mariusz Molon; Vanessa Gwildies; Roland A. Fischer
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	5808 - 5814
a	12.1447 ± 0.0003 Å
b	12.5678 ± 0.0003 Å
c	20.3119 ± 0.0005 Å
α	87.634 ± 0.002°
β	81.14 ± 0.002°
γ	64.001 ± 0.002°
Cell volume	2752.06 ± 0.13 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0389
Residual factor for significantly intense reflections	0.0302
Weighted residual factors for significantly intense reflections	0.0721
Weighted residual factors for all reflections included in the refinement	0.0763
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179357 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/54.	4325448.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4325448.cif
44518	2012-03-16	../uploads/cif-deposit/cod/cif Adding structures of 4325448 via cif-deposit CGI script.	4325448.cif