Crystallography Open Database

Information card for entry 4326381

Preview

Coordinates	4326381.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H69 Ge N7 O65 P2 W17
Calculated formula	C11 H5 Ge N4 O64 P2 W17
Title of publication	Synthesis and Structure of Dawson Polyoxometalate-Based, Multifunctional, Inorganic-Organic Hybrid Compounds: Organogermyl Complexes with One Terminal Functional Group and Organosilyl Analogues with Two Terminal Functional Groups
Authors of publication	Kenji Nomiya; Yoshihiro Togashi; Yuhki Kasahara; Shotaro Aoki; Hideaki Seki; Marie Noguchi; Shoko Yoshida
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	9606 - 9619
a	26.3455 ± 0.0019 Å
b	20.581 ± 0.0015 Å
c	15.0517 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	8161.3 ± 1 Å³
Cell temperature	90 K
Ambient diffraction temperature	90 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.064
Residual factor for significantly intense reflections	0.0532
Weighted residual factors for significantly intense reflections	0.1348
Weighted residual factors for all reflections included in the refinement	0.1416
Goodness-of-fit parameter for all reflections included in the refinement	1.127
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179366 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/63.	4326381.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4326381.cif
48545	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4326381 via cif-deposit CGI script.	4326381.cif