Crystallography Open Database

Information card for entry 4326530

Preview

Coordinates	4326530.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H40 F9 N O6 P2 S Si
Calculated formula	C20 H40 F9 N O6 P2 S Si
Title of publication	Reactions of Phosphine Oxides with Bromophosphoranimines; Synthesis and Unusual Rearrangements of O-Donor Stabilized Phosphoranimine Cations
Authors of publication	Martin Bendle; Keith Huynh; Mairi F. Haddow; Ian Manners
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	10292 - 10302
a	24.951 ± 0.0012 Å
b	17.4531 ± 0.0008 Å
c	22.1048 ± 0.0009 Å
α	90°
β	93.28 ± 0.002°
γ	90°
Cell volume	9610.3 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1888
Residual factor for significantly intense reflections	0.1028
Weighted residual factors for significantly intense reflections	0.2156
Weighted residual factors for all reflections included in the refinement	0.254
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179368 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/65.	4326530.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4326530.cif
48821	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4326530 via cif-deposit CGI script.	4326530.cif