Crystallography Open Database

Information card for entry 4327232

Preview

Coordinates	4327232.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H54 Cl8 Co2 N12 O16 P4 Zn4
Calculated formula	C12 H6 Cl8 Co2 N12 O16 P4 Zn4
Title of publication	Syntheses and Characterizations of Three Low-Dimensional Chloride-Rich Zincophosphates Assembled about [d-Co(en)3]3+ and [dl-Co(en)3]3+ Complex Cations
Authors of publication	Peng Chen; Jiyang Li; Fangzheng Duan; Jihong Yu; Ruren Xu; Raj Pal Sharma
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	6683 - 6687
a	30.989 ± 0.006 Å
b	8.96 ± 0.0018 Å
c	16.326 ± 0.003 Å
α	90°
β	100.1 ± 0.03°
γ	90°
Cell volume	4462.9 ± 1.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1045
Residual factor for significantly intense reflections	0.0726
Weighted residual factors for significantly intense reflections	0.145
Weighted residual factors for all reflections included in the refinement	0.156
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179375 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/72.	4327232.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327232.cif
60948	2012-06-20	cif/ Adding structures of 4327232 via cif-deposit CGI script.	4327232.cif